VNI synthesis
- Product Name:VNI
- CAS Number:1246770-52-4
- Molecular formula:C26H19Cl2N5O2
- Molecular Weight:504.37
![Carbamic acid, [(2,4-dichlorophenyl)methylene]-, 1,1-dimethylethyl ester (9CI)](/CAS/20210305/GIF/163226-26-4.gif)
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Yield:-
Steps:
Multi-step reaction with 5 steps
1: (1R,2R)-N1,N2-bis[4-(1-pyrrolidinyl)-2-quinolinyl]-1,2-cyclohexanediamine / toluene / 48 h / -78 - -20 °C
2: cobalt(II) chloride; sodium tetrahydroborate / methanol / 0 - 20 °C
3: ammonium acetate / methanol; water / 20 h / Reflux
4: trifluoroacetic acid / dichloromethane / 14 h / 20 °C
5: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap / dichloromethane / 0 - 20 °C
References:
Dobish, Mark C.;Villalta, Fernando;Waterman, Michael R.;Lepesheva, Galina I.;Johnston, Jeffrey N. [Organic Letters,2012,vol. 14,# 24,p. 6322 - 6325]
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