1,3-Benzodioxol-4-ylmethanol
- CAS No.
- 769-30-2
- Chemical Name:
- 1,3-Benzodioxol-4-ylmethanol
- Synonyms
- RARECHEM AL BD 0228;Benzodioxol-4-ylmethanol;1,3-Benzodioxole-4-methanol;1,3-Benzodioxol-4-ylmethanol;2H-1,3-benzodioxol-4-ylMethanol;(benzo[d][1,3]dioxol-4-yl）methanol;2,3-(Methylenedioxy)benzyl alcohol;4-(Hydroxymethyl)-1,3-benzodioxole;(1,3-Benzodioxol-4-yl)methanol, 2,3-(Methylenedioxy)benzyl alcohol
- CBNumber:
- CB1381065
- Molecular Formula:
- C8H8O3
- Molecular Weight:
- 152.15
- MDL Number:
- MFCD02681980
- MOL File:
- 769-30-2.mol
- MSDS File:
- SDS
| Melting point | 39℃ |
|---|---|
| Boiling point | 124 °C |
| Density | 1.329±0.06 g/cm3 (20 ºC 760 Torr) |
| Flash point | 127.9±21.5℃ |
| storage temp. | Inert atmosphere,Room Temperature |
| pka | 14.24±0.10(Predicted) |
| InChI | InChI=1S/C8H8O3/c9-4-6-2-1-3-7-8(6)11-5-10-7/h1-3,9H,4-5H2 |
| InChIKey | XVCMMPXFVAHHQN-UHFFFAOYSA-N |
| SMILES | O1C2=CC=CC(CO)=C2OC1 |
| CAS DataBase Reference | 769-30-2 |
SAFETY
Risk and Safety Statements
| Symbol(GHS) |  GHS07 |
|---|---|
| Signal word | Warning |
| Hazard statements | H302+H312+H332-H315-H319 |
| Precautionary statements | P501-P261-P270-P271-P264-P280-P337+P313-P305+P351+P338-P362+P364-P332+P313-P301+P312+P330-P302+P352+P312-P304+P340+P312 |
| Safety Statements | 24/25 |
| HS Code | 2932990090 |
1,3-Benzodioxol-4-ylmethanol price More Price(45)
| Manufacturer | Product number | Product description | CAS number | Packaging | Price | Updated | Buy |
|---|---|---|---|---|---|---|---|
| Activate Scientific | AS38904 | Benzo[d][1,3]dioxol-4-ylmethanol 97% | 769-30-2 | 1g | $52 | 2026-06-04 | Buy |
| Activate Scientific | AS38904 | Benzo[d][1,3]dioxol-4-ylmethanol 97% | 769-30-2 | 5g | $157 | 2026-06-04 | Buy |
| Activate Scientific | AS38904 | Benzo[d][1,3]dioxol-4-ylmethanol 97% | 769-30-2 | 25g | $455 | 2026-06-04 | Buy |
| Matrix Scientific | 222096 | Benzo[d][1,3]dioxol-4-ylmethanol | 769-30-2 | 10.00g | $318 | 2026-05-18 | Buy |
| Matrix Scientific | 222096 | Benzo[d][1,3]dioxol-4-ylmethanol | 769-30-2 | 25.00g | $635 | 2026-05-18 | Buy |
1,3-Benzodioxol-4-ylmethanol Chemical Properties, Uses, Production
Synthesis
33842-16-9
769-30-2
General procedure for the synthesis of 1,3-benzodioxolane-4-alkylmethanol from methyl benzo[d][1,3]meso-dioxolane-4-carboxylate: 6.7 g (0.037 mol) of methyl benzo[d][1,3]meso-dioxolane-4-carboxylate was dissolved in 50 mL of tetrahydrofuran and 8.6 g (0.223 mol) of sodium borohydride was added. The temperature of the reaction system was raised to 65 °C and the reaction was continuously stirred for 30 min. Heating and stirring were stopped and 8 mL of methanol was added slowly and dropwise over 30 minutes. A large number of bubbles were observed to be generated during the reaction, after which the reaction mixture was refluxed for 4 hours. Upon completion of the reaction, the reaction was quenched with saturated ammonium chloride solution, the reaction mixture was filtered and the tetrahydrofuran was removed by distillation under reduced pressure. Ethyl acetate was added to the residue to partition the organic and aqueous phases, and the organic phase was washed with saturated brine and dried with anhydrous sodium sulfate for 8 hours. The desiccant was removed by filtration and the solvent was evaporated under reduced pressure to give 5.6 g of a white oily product, 1,3-benzodioxolane-4-alkylmethanol. Thin layer chromatography (TLC) analysis showed a single spot and the purity of the product met the requirements for subsequent reactions. The yield was close to 100%.
References
[1] Patent: CN103804341, 2018, B. Location in patent: Paragraph 0064; 0070; 0071
[2] Chemische Berichte, 1958, vol. 91, p. 36,38
1,3-Benzodioxol-4-ylmethanol Preparation Products And Raw materials
Raw materials
Preparation Products
1,3-Benzodioxol-4-ylmethanol Suppliers
| Supplier | Tel | Country | ProdList | Advantage | |
|---|---|---|---|---|---|
| Shijiazhuang Tancheng Biological Technology Co., Ltd | 0311-84309789 13833149888 | tanchengchem@163.com | China | 36 | 58 |
| J & K SCIENTIFIC LTD. | 18210857532 18210857532 | jkinfo@jkchemical.com | China | 96815 | 76 |
| JinYan Chemicals(ShangHai) Co.,Ltd. | 13817811078 | sales@jingyan-chemical.com | China | 9963 | 60 |
| Nanjing Chemlin Chemical Co., Ltd | 025-83697070 13770331960 | info@chemlin.com.cn | China | 16305 | 64 |
| Shanghai Hanhong Scientific Co.,Ltd. | 021-54306202 13764082696 | info@hanhongsci.com | China | 42917 | 64 |
| Shanghai Sunway Pharmaceutical Technology Co., Ltd | 13761987713 | hxzheng@sunwaypharm.cn | China | 8663 | 57 |
| Hunan Hui Bai Shi Biotechnology Co., Ltd. | 0731-85526065 13308475853 | ivy@hnhbsj.com | China | 7236 | 62 |
| T&W GROUP | 021-61551611 13296011611 | contact@trustwe.com | China | 9884 | 58 |
| Thermo Fisher Scientific | 800-810-5118 | cnchemical@thermofisher.com | China | 17752 | 75 |
| Shanghai T&W Pharmaceutical Co., Ltd. | +86 21 61551611 | China | 9874 | 58 |
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