5,5'-Dibromo-2,2'-bipyridyl
- CAS No.
- 15862-18-7
- Chemical Name:
- 5,5'-Dibromo-2,2'-bipyridyl
- Synonyms
- EA793;5-Dibromo-2;2-bipyridyl;5,5'-dibromo-2,2'-dipyridyl;5,5'-Dibromo-2,2'-bipyridyl;5,5'-dibromo-2,2'-bipyridine;2,2'-Bipyridine,5,5'-dibroMo-;5,5'-Dibromo-2,2'-bipyridyl>5-Bromo-2-(5-bromo-2-pyridyl)pyridine;5-bromo-2-(5-bromopyridin-2-yl)pyridine
- CBNumber:
- CB61177167
- Molecular Formula:
- C10H6Br2N2
- Molecular Weight:
- 313.98
- MDL Number:
- MFCD06657883
- MOL File:
- 15862-18-7.mol
- MSDS File:
- SDS
| Product description | Number | Pack Size | Price |
| 5,5'-Dibromo-2,2'-bipyridyl >98.0%(HPLC) | D4358 | 1g | $155 |
| 5,5'-Dibromo-2,2'-bipyridyl | FD30037 | 1g | $160 |
| 5,5'-Dibromo-2,2'-bipyridyl,≥98%(HPLC) ≥98%(HPLC) | 31824 | 1G | $192.19 |
| 5,5'-Dibromo-2,2'-bipyridine | 7964AA | 1g | $252 |
| 5,5'-Dibromo-2,2'-bipyridyl | FD30037 | 250mg | $60 |
| More product size | |||
| Melting point | 225.0 to 229.0 °C |
|---|---|
| Boiling point | 358℃ |
| Density | 1.809 |
| Flash point | 170℃ |
| storage temp. | Sealed in dry,Room Temperature |
| pka | 1.49±0.32(Predicted) |
| form | powder to crystal |
| color | White to Almost white |
| InChI | InChI=1S/C10H6Br2N2/c11-7-1-3-9(13-5-7)10-4-2-8(12)6-14-10/h1-6H |
| InChIKey | JNWPRPLNUUMYCM-UHFFFAOYSA-N |
| SMILES | C1(C2=NC=C(Br)C=C2)=NC=C(Br)C=C1 |
SAFETY
Risk and Safety Statements
| Symbol(GHS) |  GHS07 |
|---|---|
| Signal word | Warning |
| Hazard statements | H315-H319 |
| Precautionary statements | P264-P280-P302+P352+P332+P313+P362+P364-P305+P351+P338+P337+P313 |
| Safety Statements | 24/25 |
| HS Code | 29333990 |
5,5'-Dibromo-2,2'-bipyridyl price More Price(34)
| Manufacturer | Product number | Product description | CAS number | Packaging | Price | Updated | Buy |
|---|---|---|---|---|---|---|---|
| TCI Chemical | D4358 | 5,5'-Dibromo-2,2'-bipyridyl >98.0%(HPLC) | 15862-18-7 | 1g | $155 | 2025-07-31 | Buy |
| Biosynth Carbosynth | FD30037 | 5,5'-Dibromo-2,2'-bipyridyl | 15862-18-7 | 1g | $160 | 2021-12-16 | Buy |
| Chem-Impex | 31824 | 5,5'-Dibromo-2,2'-bipyridyl,≥98%(HPLC) ≥98%(HPLC) | 15862-18-7 | 1G | $192.19 | 2021-12-16 | Buy |
| AK Scientific | 7964AA | 5,5'-Dibromo-2,2'-bipyridine | 15862-18-7 | 1g | $252 | 2021-12-16 | Buy |
| Biosynth Carbosynth | FD30037 | 5,5'-Dibromo-2,2'-bipyridyl | 15862-18-7 | 250mg | $60 | 2021-12-16 | Buy |
5,5'-Dibromo-2,2'-bipyridyl Chemical Properties,Uses,Production
Uses
5,5''-Dibromo-2,2''-bipyridine
Synthesis
366-18-7
15862-18-7
The general procedure for the synthesis of 5,5'-dibromo-2,2'-bipyridine from 2,2'-bipyridine was as follows: firstly, 2,2'-bipyridine (4.99 g, 0.032 mol) was placed in a hydrothermal reactor with bromine (10.24 g, 0.064 mol), and the reaction was heated up to 150 °C for 15 hours. Upon completion of the reaction, the mixture was cooled to room temperature and the resulting solid product was pulverized and washed with Na2SO3 solution to remove unreacted bromine. Subsequently, the reaction mixture was alkalized with sodium hydroxide solution and the solid product was collected by filtration. Purification by silica gel column chromatography (eluent: CH2Cl2) afforded 5,5'-dibromo-2,2'-bipyridine as a white solid (8.64 g, 86% yield). The melting point of the product was 221.6-222.1°C. 1H-NMR (400 MHz, CDCl3, δ): 7.95 (d, 2H), 8.28 (s, 2H), 8.71 (d, 2H); 13C-NMR (100 MHz, CDCl3, δ): 121.47 (C5), 122.25 (C3), 139.64 (C4 ), 150.28 (C6), 153.64 (C2); IR (KBr, cm-1): 3049 (C-H stretching vibration), 1562, 1453, 1356 (aromatic ring stretching vibration), 636 (C-Br stretching vibration). Elemental analysis (C10H6N2Br2) calculated values: C 38.22%, H 1.91%, N 8.92%, Br 50.95%; measured values: C 38.26%, H 1.94%, N 8.90%, Br 50.97%.
References
[1] Reactive and Functional Polymers, 2016, vol. 106, p. 93 - 98
[2] Patent: CN105130885, 2018, B. Location in patent: Paragraph 0024; 0026; 0027; 0030; 0033; 0036
[3] New Journal of Chemistry, 2018, vol. 42, # 17, p. 14067 - 14070
[4] Chemistry - A European Journal, 2015, vol. 21, # 51, p. 18576 - 18579
[5] Patent: WO2009/118742, 2009, A1
5,5'-Dibromo-2,2'-bipyridyl Preparation Products And Raw materials
Raw materials
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Preparation Products
| Supplier | Tel | Country | ProdList | Advantage | |
|---|---|---|---|---|---|
| Shanghai UCHEM Inc. | +862156762820 +86-13564624040 | sales@myuchem.com | China | 8566 | 58 |
| ATK CHEMICAL COMPANY LIMITED | +undefined-21-51877795 | ivan@atkchemical.com | China | 33024 | 60 |
| career henan chemical co | +86-0371-86658258 +8613203830695 | sales@coreychem.com | China | 29837 | 58 |
| Shenzhen Nexconn Pharmatechs Ltd | +86-755-89396905 +86-15013857715 | admin@nexconn.com | China | 10405 | 58 |
| Jilin Chinese Academy of Sciences - Yanshen Technology Co., Ltd. | 0431-80514535 13634302652 | Extension@chemextension.com | CHINA | 967 | 58 |
| Accela ChemBio Inc. | +1-858-6993322 | info@accelachem.com | United States | 21193 | 58 |
| Shandong chuangyingchemical Co., Ltd. | 18853181302 | sale@chuangyingchem.com | CHINA | 5906 | 58 |
| Alchem Pharmtech,Inc. | 8485655694 | sales@alchempharmtech.com | United States | 63687 | 58 |
| CHEMSOON CO.,LTD. | +8613761723174 | sales01@chemsoon.com | China | 1211 | 58 |
| Zhengzhou Alfa Chemical Co.,Ltd | +8618530059196 | sale04@alfachem.cn | China | 11732 | 58 |
View Lastest Price from 5,5'-Dibromo-2,2'-bipyridyl manufacturers
| Image | Update time | Product | Price | Min. Order | Purity | Supply Ability | Manufacturer | |
|---|---|---|---|---|---|---|---|---|
 |
2026-01-16 | 5,5'-Dibromo-2,2'-bipyridine
15862-18-7
|
US $20.00-201.00 / g | 1g | 0.98 | 25kg | Shanghai UCHEM Inc. | |
 |
2019-07-06 | 5,5'-Dibromo-2,2'-bipyridyl
15862-18-7
|
US $1.00 / KG | 1G | 98% | 1000KG | Career Henan Chemical Co |
-
- 5,5'-Dibromo-2,2'-bipyridine
15862-18-7
- US $20.00-201.00 / g
- 0.98
- Shanghai UCHEM Inc.
-
- 5,5'-Dibromo-2,2'-bipyridyl
15862-18-7
- US $1.00 / KG
- 98%
- Career Henan Chemical Co
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