2',3'-Dimethoxyacetophenone
- CAS No.
- 38480-94-3
- Chemical Name:
- 2',3'-Dimethoxyacetophenone
- Synonyms
- 1-(2,3-Dimethoxyphenyl)ethan-1-one;2',3'-Dimethoxyacetophenone;2',3'-Dimethoxyacetophenone;Ethanone, 1-(2,3-diMethoxyphenyl)-;2-Methoxy-1-(3-Methoxyphenyl)ethan-1-one
- CBNumber:
- CB7174991
- Molecular Formula:
- C10H12O3
- Molecular Weight:
- 180.2
- MDL Number:
- MFCD03424412
- MOL File:
- 38480-94-3.mol
- MSDS File:
- SDS
| Melting point | 29.5-51.5℃ |
|---|---|
| Boiling point | 156-158℃ |
| Density | 1.066±0.06 g/cm3(Predicted) |
| storage temp. | Sealed in dry,Room Temperature |
| form | solid |
| Appearance | Light yellow to brown Liquid |
| InChI | 1S/C10H12O3/c1-7(11)8-5-4-6-9(12-2)10(8)13-3/h4-6H,1-3H3 |
| InChIKey | FODUVZQSLRHUMC-UHFFFAOYSA-N |
| SMILES | COc1cccc(C(C)=O)c1OC |
| UNSPSC Code | 12352200 |
| NACRES | NA.21 |
SAFETY
Risk and Safety Statements
| Symbol(GHS) |  GHS07 |
|---|---|
| Signal word | Warning |
| Hazard statements | H302-H319 |
| Precautionary statements | P301+P312+P330-P305+P351+P338 |
| WGK Germany | WGK 3 |
| HS Code | 2914500090 |
| Storage Class | 11 - Combustible Solids |
| Hazard Classifications | Acute Tox. 4 Oral Eye Irrit. 2 |
2',3'-Dimethoxyacetophenone price More Price(39)
| Manufacturer | Product number | Product description | CAS number | Packaging | Price | Updated | Buy |
|---|---|---|---|---|---|---|---|
| Sigma-Aldrich | IDF00009 | 2′,3′-Dimethoxyacetophenone Aldrich | 38480-94-3 | 1g | $352 | 2026-04-30 | Buy |
| Apolloscientific | OR938335 | 2',3'-Dimethoxyacetophenone 97% | 38480-94-3 | 250mg | $21 | 2026-06-04 | Buy |
| Apolloscientific | OR938335 | 2',3'-Dimethoxyacetophenone 97% | 38480-94-3 | 1g | $22 | 2026-06-04 | Buy |
| Apolloscientific | OR938335 | 2',3'-Dimethoxyacetophenone 97% | 38480-94-3 | 5g | $102 | 2026-06-04 | Buy |
| Apolloscientific | OR938335 | 2',3'-Dimethoxyacetophenone 97% | 38480-94-3 | 25g | $485 | 2026-06-04 | Buy |
2',3'-Dimethoxyacetophenone Chemical Properties, Uses, Production
Uses
2'',3''-Dimethoxyacetophenone is used as a reactant in the preparation and antileishmanial activity of quinazolinone hybrids.
Preparation
Obtained by heating its oxime with pyridinium chloride containing 5% of water (35%).
Synthesis
6848-73-3
38480-94-3
General procedure for the synthesis of 2,3-dimethoxyacetophenone from 1-(2,3-dimethoxyphenyl)ethanol: Potassium dichromate (24.76 g), water (124 mL), and concentrated sulfuric acid (12 mL) were prepared into a solution, and 1-(2,3-dimethoxyphenyl)ethanol (10.06 g, 55.3 mmol) was added, and the reaction was stirred for 15 min at room temperature. After completion of the reaction, the reaction mixture was extracted with ether and the organic phase was washed sequentially with 5% potassium carbonate solution (2 x 150 mL) and saturated sodium chloride solution (1 x 100 mL). The organic phase was dried and the solvent was evaporated under reduced pressure to obtain the crude product. The crude product was purified by high-vacuum distillation and collected at a pressure of 0.3 Torr and a temperature of 85 °C to give 6.47 g of 2,3-dimethoxyacetophenone in 65% yield. The 1H NMR (300 MHz, CDCl3) data of the product were as follows: δ 2.62 (s, 3H), 3.88 (s, 3H), 3.90 (s, 3H), 7.05-7.10 (m, 2H), 7.21 (dd, 1H).
References
[1] Patent: US5990142, 1999, A
[2] Journal of the American Chemical Society, 1951, vol. 73, p. 793
[3] Chemische Berichte, 1913, vol. 46, p. 4019
[4] Journal of the American Chemical Society, 2005, vol. 127, # 29, p. 10371 - 10387
2',3'-Dimethoxyacetophenone Preparation Products And Raw materials
| Supplier | Tel | Country | ProdList | Advantage | |
|---|---|---|---|---|---|
| Jia Xing Isenchem Co.,Ltd | 0573-85285100 18627885956 | isenchem@163.com | China | 9389 | 66 |
| Shanghai Harvest Chemical Industrial Co., Ltd. | 15721252604 17321035817 | sales@harvest-chem.com | China | 2829 | 64 |
| Chengdu HappySyn Pharmaceutical Technology Co., Ltd. | 85114309 18982182443 | yangli@happysyn.com | China | 2297 | 55 |
| Shanghai Topbiochem Technology Co., Ltd | 021-58170097 | info@topbiochem.com | China | 9509 | 58 |
| Shanghai Yolne Chemical Co., Ltd. | 021-62960152 | 934678158@qq.com | China | 9886 | 55 |
| Bide Pharmatech Ltd. | 400-164-7117 18317119277 | product02@bidepharm.com | China | 40000 | 60 |
| Finetech Industry Limited | 027-87465837 19945049750 | sales@finetechnology-ind.com | China | 9331 | 58 |
| ShangHai KenEn Chemical Technology Co., Ltd. | 13120367189;18621755571 | mychess007@163.com | China | 1994 | 55 |
| Tianjin Anhao Biological Technology Co., Ltd. | sales@ahpharmatech.com | China | 5734 | 55 | |
| Cool Pharm, Ltd | 021-60455363 18019463053 | sales@coolpharm.com | China | 8455 | 58 |
View Latest Price from 2',3'-Dimethoxyacetophenone manufacturers
| Image | Update time | Product | Price | Min. Order | Purity | Supply Ability | Manufacturer | |
|---|---|---|---|---|---|---|---|---|
 |
2020-01-10 | Ethanone, 1-(2,3-dimethoxyphenyl)-
38480-94-3
|
1KG | 98%; 99% | 500g;1kg； 25kg | Career Henan Chemical Co |
-
- Ethanone, 1-(2,3-dimethoxyphenyl)-
38480-94-3
- $0.01
- 98%; 99%
- Career Henan Chemical Co
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