2-Methoxy-6-methylbenzaldehyde
- CAS No.
- 54884-55-8
- Chemical Name:
- 2-Methoxy-6-methylbenzaldehyde
- Synonyms
- 6-Methoxy-2-methylbenzaldehyde;2-Methoxy-6-methylbenzaldehyde;Benzaldehyde, 2-Methoxy-6-Methyl-
- CBNumber:
- CB7225811
- Molecular Formula:
- C9H10O2
- Molecular Weight:
- 150.17
- MDL Number:
- MFCD08235006
- MOL File:
- 54884-55-8.mol
- MSDS File:
- SDS
SAFETY
Risk and Safety Statements
| Symbol(GHS) |  GHS07 |
|---|---|
| Signal word | Warning |
| Hazard statements | H315-H319-H335 |
| Precautionary statements | P261-P305+P351+P338 |
| HS Code | 2912490090 |
2-Methoxy-6-methylbenzaldehyde price More Price(36)
| Manufacturer | Product number | Product description | CAS number | Packaging | Price | Updated | Buy |
|---|---|---|---|---|---|---|---|
| Apolloscientific | OR18418 | 2-Methoxy-6-methylbenzaldehyde 97% | 54884-55-8 | 100mg | $21 | 2026-06-04 | Buy |
| Apolloscientific | OR18418 | 2-Methoxy-6-methylbenzaldehyde 97% | 54884-55-8 | 250mg | $24 | 2026-06-04 | Buy |
| Apolloscientific | OR18418 | 2-Methoxy-6-methylbenzaldehyde 97% | 54884-55-8 | 1g | $56 | 2026-06-04 | Buy |
| Apolloscientific | OR18418 | 2-Methoxy-6-methylbenzaldehyde 97% | 54884-55-8 | 5g | $264 | 2026-06-04 | Buy |
| Activate Scientific | AS39374 | 2-Methoxy-6-methylbenzaldehyde 97% | 54884-55-8 | 1g | $51 | 2026-06-04 | Buy |
2-Methoxy-6-methylbenzaldehyde Chemical Properties, Uses, Production
Synthesis Reference(s)
Synthesis, p. 1000, 1983 DOI: 10.1055/s-1983-30599
Synthesis
2944-49-2
54884-55-8
General procedure for the synthesis of 2-methoxy-6-methylbenzaldehyde from 1-methoxy-2,3-dimethylbenzene: Potassium peroxydisulfate (89.31 g, 0.33 mol) and copper(II) sulfate pentahydrate (27.22 g, 0.11 mol) were added to a mixture of 1-methoxy-2,3-dimethylbenzene (15 g, 0.11 mol) in aqueous acetonitrile ( 750 mL, V/V=1:1). The reaction mixture was stirred under reflux conditions for 15 minutes until complete consumption of the feedstock was confirmed by thin layer chromatography (TLC) detection. Upon completion of the reaction, the mixture was cooled to room temperature and the product was extracted with dichloromethane (2 x 225 mL). The organic layers were combined and washed sequentially with water (2 x 100 mL) and saturated saline (100 mL). The organic layer was dried over anhydrous sodium sulfate and concentrated under reduced pressure to obtain the crude product. The crude product was purified by silica gel column chromatography with the eluent of 4/96 (V/V) ethyl acetate/hexane to afford 2-methoxy-6-methylbenzaldehyde (7.32 g, 44.2% yield). The structure of the product was confirmed by 1H NMR (300 MHz, CDCl3): δ 2.60 (3H, s), 3.90 (3H, s), 6.80 (2H, t), 7.40 (1H, t), 10.65 (1H, s).
References
[1] Tetrahedron, 1996, vol. 52, # 6, p. 2199 - 2216
[2] Chemical Communications, 2013, vol. 49, # 77, p. 8626 - 8628
[3] Angewandte Chemie - International Edition, 2013, vol. 52, # 2, p. 762 - 766
[4] Angew. Chem., 2013, vol. 125, # 2, p. 791 - 796,6
[5] Chemistry - A European Journal, 2015, vol. 21, # 29, p. 10322 - 10325
2-Methoxy-6-methylbenzaldehyde Preparation Products And Raw materials
Raw materials
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Preparation Products
2-Methoxy-6-methylbenzaldehyde Suppliers
| Supplier | Tel | Country | ProdList | Advantage | |
|---|---|---|---|---|---|
| Adamas Reagent, Ltd. | 400-6009262 15618770481 | yhx@titansci.com | China | 14098 | 59 |
| Beijing Eternalchem Co,. Ltd. | 010-59484199 18611897322;18611897322; | sales@eternalchem.com | China | 1993 | 60 |
| Hangzhou Sage Chemical Co., Ltd. | +86057186818502 13588463833 | info@sagechem.com | China | 10265 | 58 |
| SynAsst Chemical. | 021-60343070 | China | 12731 | 55 | |
| Shanghai Run-Biotech Co., Ltd. | 021-57171705 13817537615 | sales@run-biotech.com | China | 2283 | 58 |
| Bide Pharmatech Ltd. | 400-164-7117 18317119277 | product02@bidepharm.com | China | 40000 | 60 |
| Shanghai HuanChuan Industry Co.,Ltd. | 021-61478794 | sales@hcshhai.com | China | 9781 | 50 |
| Hangzhou Milestone Pharmtech Co., Ltd. | 0571-82896630 18969958410 | sales_hz@milestonepharmtech.com | China | 4906 | 55 |
| ShangHai Angti Biotechnology Co., Ltd. | 13764913901 | info@angtibio.com | China | 4975 | 55 |
| Shanghai YuanYe Biotechnology Co., Ltd. | 15026964105 | 2881489226@qq.com | China | 89667 | 60 |
View Latest Price from 2-Methoxy-6-methylbenzaldehyde manufacturers
| Image | Update time | Product | Price | Min. Order | Purity | Supply Ability | Manufacturer | |
|---|---|---|---|---|---|---|---|---|
 |
2020-01-05 | 2-METHOXY-6-METHYLBENZALDEHYDE
54884-55-8
|
$9.80 | 1KG | 97%-99% | 1kg -1000kg | Career Henan Chemical Co |
-
- 2-METHOXY-6-METHYLBENZALDEHYDE
54884-55-8
- $9.80
- 97%-99%
- Career Henan Chemical Co
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