N-phenyl isonicotinamide
- CAS No.
- 3034-31-9
- Chemical Name:
- N-phenyl isonicotinamide
- Synonyms
- SKL864;NSC 4266;Isonicotinanilide;N-Phenyl isonicotinicamide;1,2-Ethanediamine,4-phenyl-;N-Phenyl isonicotinamide ,97%;4-(N-Phenylcarbamoyl)pyridine;N-Phenyl-4-pyridinecarboxamide;N-phenylpyridine-4-carboxamide;4-Pyridinecarboxamide,N-phenyl-
- CBNumber:
- CB7950393
- Molecular Formula:
- C12H10N2O
- Molecular Weight:
- 198.22
- MDL Number:
- MFCD00459246
- MOL File:
- 3034-31-9.mol
- MSDS File:
- SDS
| Product description | Number | Pack Size | Price |
| N-PHENYL-ISONICOTINAMIDE 97% | 65128 | 1G | $27 |
| N-PHENYL-ISONICOTINAMIDE 97% | 65128 | 5G | $69 |
| N-PHENYL-ISONICOTINAMIDE 97% | 65128 | 25G | $299 |
| N-Phenylisonicotinamide >98% | OR904044 | 1g | $21 |
| N-Phenylisonicotinamide >98% | OR904044 | 5g | $39 |
| More product size | |||
SAFETY
Risk and Safety Statements
| Symbol(GHS) |   GHS06,GHS08 |
|---|---|
| Signal word | Danger |
| Hazard statements | H301-H315-H319-H341 |
| Precautionary statements | P501-P270-P202-P201-P264-P280-P302+P352-P308+P313-P337+P313-P305+P351+P338-P362+P364-P332+P313-P301+P310+P330-P405 |
| HS Code | 29333990 |
N-phenyl isonicotinamide price More Price(34)
| Manufacturer | Product number | Product description | CAS number | Packaging | Price | Updated | Buy |
|---|---|---|---|---|---|---|---|
| AstaTech | 65128 | N-PHENYL-ISONICOTINAMIDE 97% | 3034-31-9 | 1G | $27 | 2026-04-30 | Buy |
| AstaTech | 65128 | N-PHENYL-ISONICOTINAMIDE 97% | 3034-31-9 | 5G | $69 | 2026-04-30 | Buy |
| AstaTech | 65128 | N-PHENYL-ISONICOTINAMIDE 97% | 3034-31-9 | 25G | $299 | 2026-04-30 | Buy |
| Apolloscientific | OR904044 | N-Phenylisonicotinamide >98% | 3034-31-9 | 1g | $21 | 2026-06-04 | Buy |
| Apolloscientific | OR904044 | N-Phenylisonicotinamide >98% | 3034-31-9 | 5g | $39 | 2026-06-04 | Buy |
N-phenyl isonicotinamide Chemical Properties,Uses,Production
Chemical Properties
White to light yellow or grey solid
Synthesis
55-22-1
62-53-3
3034-31-9
General procedure for the synthesis of N-phenylisonicotinamide from isonicotinic acid and aniline: isonicotinic acid (14.5 g, 40.6 mmol) was dissolved in thionyl chloride (40 mL) and heated to reflux for 2 hours. After completion of the reaction, thionyl chloride was removed by distillation under reduced pressure. To the residue was added THF (50 mL), K2CO3 (16.8 g, 121.9 mmol) and aniline (3.78 g, 40.6 mmol), and the reaction mixture was stirred at room temperature for 24 hours. After completion of the reaction, the reaction mixture was diluted with water (100 mL) and extracted with EtOAc (2 x 100 mL). The organic layers were combined, concentrated, and the residue was recrystallized with EtOAc-hexane (60:40) to afford the light yellow solid product N-phenylisonicotinamide (8.0 g, 99% yield) with melting point 166-168 °C. IR (KBr) νmax 1344, 1653, 1465, 665 cm-1 ; 1H NMR (DMSO-d6, 300 MHz) δ 10.49 (s, 1H), 8.78 (m, 2H), 7.86 (m, 2H), 7.78 (m, 2H), 7.39 (t, J = 8.0 Hz, 2H), 7.15 (t, J = 6.5 Hz, 1H).
References
[1] Patent: WO2017/160898, 2017, A1. Location in patent: Paragraph 00105; 00125
[2] Journal of Medicinal Chemistry, 2016, vol. 59, # 4, p. 1370 - 1387
[3] Bioorganic and Medicinal Chemistry, 2008, vol. 16, # 11, p. 6027 - 6033
[4] Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1981, vol. 20, # 11, p. 1007 - 1008
N-phenyl isonicotinamide Preparation Products And Raw materials
Raw materials
1of2
Preparation Products
| Supplier | Tel | Country | ProdList | Advantage | |
|---|---|---|---|---|---|
| Capot Chemical Co.,Ltd. | +86-（0）57185586718 +86-13336195806 | sales@capot.com | China | 29626 | 60 |
| ATK CHEMICAL COMPANY LIMITED | +undefined-21-51877795 | ivan@atkchemical.com | China | 32998 | 60 |
| Alchem Pharmtech,Inc. | 8485655694 | sales@alchempharmtech.com | United States | 63645 | 58 |
| Fuxin Pharmaceutical | +86-021-021-50872116 | contact@fuxinpharm.com | China | 9976 | 58 |
| Hefei TNJ Chemical Industry Co.,Ltd. | +86-0551-65418671 +86-189 4982 3763 | sales@tnjchem.com | China | 34526 | 58 |
| Dayang Chem (Hangzhou) Co.,Ltd. | +86-0571-88938639 17705817739 | info@dycnchem.com | China | 52693 | 58 |
| Hong Kong Tiansheng New Material Trading Co., Ltd | +8617320695765 | zxx@hktiansheng.com | China | 967 | 58 |
| Labnetwork lnc. | +86-27-50766799 +86-18062016861 | contact@labnetwork.com | China | 19981 | 58 |
| Aromsyn Co., Ltd. | +86-0571-85585865 +86-13336024896 | CB@aromsyn.com | China | 19176 | 58 |
| PT CHEM GROUP LIMITED | +86-85511178; +86-85511178 | peter68@ptchemgroup.com | China | 35405 | 58 |
View Lastest Price from N-phenyl isonicotinamide manufacturers
| Image | Update time | Product | Price | Min. Order | Purity | Supply Ability | Manufacturer | |
|---|---|---|---|---|---|---|---|---|
 |
2022-02-25 | Isonicotinanilide
3034-31-9
|
$4.60 | 1KG | 99% | 100KG | Hong Kong Tiansheng New Material Trading Co., Ltd | |
 |
2022-02-25 | N-phenylpyridine-4-carboxamide
3034-31-9
|
$4.60 | 1KG | 98% | 10KG | Hong Kong Tiansheng New Material Trading Co., Ltd | |
 |
2022-02-25 | N-Phenylisonicotinamide
3034-31-9
|
$4.60 | 1KG | 99% | 10kg | Hong Kong Tiansheng New Material Trading Co., Ltd |
-
- Isonicotinanilide
3034-31-9
- $4.60
- 99%
- Hong Kong Tiansheng New Material Trading Co., Ltd
-
- N-phenylpyridine-4-carboxamide
3034-31-9
- $4.60
- 98%
- Hong Kong Tiansheng New Material Trading Co., Ltd
-
- N-Phenylisonicotinamide
3034-31-9
- $4.60
- 99%
- Hong Kong Tiansheng New Material Trading Co., Ltd
