4-아세틸-피페리딘-1-카르복실산TERT-부틸에스테르
|
|
4-아세틸-피페리딘-1-카르복실산TERT-부틸에스테르 속성
- 끓는 점
- 312.4±35.0 °C(Predicted)
- 밀도
- 1.052±0.06 g/cm3(Predicted)
- 저장 조건
- Keep in dark place,Sealed in dry,Room Temperature
- 산도 계수 (pKa)
- -2.23±0.40(Predicted)
- 물리적 상태
- solid
- 외관
- Colorless to off-white Liquid
- InChI
- InChI=1S/C12H21NO3/c1-9(14)10-5-7-13(8-6-10)11(15)16-12(2,3)4/h10H,5-8H2,1-4H3
- InChIKey
- HNVBBNZWMSTMAZ-UHFFFAOYSA-N
- SMILES
- N1(C(OC(C)(C)C)=O)CCC(C(C)=O)CC1
안전
- 위험 및 안전 성명
- 위험 및 사전주의 사항 (GHS)
4-아세틸-피페리딘-1-카르복실산TERT-부틸에스테르 C화학적 특성, 용도, 생산
용도
tert-Butyl 4-Acetylpiperidine-1-carboxylate is a useful research chemical.Synthesis
Tert-butyl-4-(methoxy(methyl)carbamoyl)piperidine-1-carboxylate (2.29 g, 8.32 mmol) was dissolved in 30 ml of tetrahydrofuran (THF), and the resulting solution was cooled to -78 °C. To the solution, methylmagnesium bromide (3.0 M) (7.73 ml, 10.82 mmol) was slowly added, and the solution was stirred at 0 °C for 1 hr. After the reaction was completed with a 2 N hydrochloric acid aqueous solution, 6 N sodium hydroxide solution was added to adjust the pH to 10. Then the solution was extracted with dichloromethane. The organic layer was treated with magnesium sulfate (MgSO4) and filtered, and the solution was concentrated. The resulting residue was isolated and purified by silica gel column chromatography (dichloromethane/methanol = 10/1) to give 4-Acetyl-piperidine-1-carboxylic acid tert-butyl ester (6.36 g, 94.0 percent).4-아세틸-피페리딘-1-카르복실산TERT-부틸에스테르 준비 용품 및 원자재
원자재
준비 용품
4-아세틸-피페리딘-1-카르복실산TERT-부틸에스테르 공급 업체
글로벌( 228)공급 업체
| 공급자 | 전화 | 이메일 | 국가 | 제품 수 | 이점 |
|---|---|---|---|---|---|
| Shanxi Tihondan Pharmaceutical Technology Co., Ltd | +8618235132063 |
sales@tihondan.com | China | 3767 | 58 |
| ZHENGZHOU JIUYI TIME NEW MATERIALS CO,.LTD | +86-13017695106 +86-13676922317 |
jiuyitime@fdachem.com | China | 9029 | 58 |
| Capot Chemical Co.,Ltd. | +86-（0）57185586718; +8613336195806 |
sales@capot.com | China | 29734 | 60 |
| Beijing Cooperate Pharmaceutical Co.,Ltd | 010-60279497 |
sales01@cooperate-pharm.com | CHINA | 1803 | 55 |
| ATK CHEMICAL COMPANY LIMITED | +undefined-21-51877795 |
ivan@atkchemical.com | China | 33024 | 60 |
| career henan chemical co | +86-0371-86658258 +8613203830695 |
sales@coreychem.com | China | 29852 | 58 |
| Jinan Carbotang Biotech Co.,Ltd. | +8615866703830 |
figo.gao@foxmail.com | China | 8497 | 58 |
| Accela ChemBio Inc. | +1-858-6993322 |
info@accelachem.com | United States | 21193 | 58 |
| Changzhou Ditong Chemical Co.,Ltd | +86-0519-88299272 |
info@edengenechem.com | China | 2176 | 58 |
| Shandong chuangyingchemical Co., Ltd. | 18853181302 |
sale@chuangyingchem.com | CHINA | 5906 | 58 |
4-아세틸-피페리딘-1-카르복실산TERT-부틸에스테르 관련 검색:
2-OXO-2,5-DIHYDRO-PYRROLE-1-CARBOXYLICACIDTERT-부틸에스테르 tert-부틸4-옥소헥사히드로시클로펜타[c]피롤-2(1H)-카르복실레이트 3-아미노-1-[(1,1-디메틸레톡시)카르보닐]-3-피페리딘아세트산메틸에스테르 1-Boc-4-시아노피페리딘 1-Boc-헥사하이드로-1H-아제핀-4-아민 프로판디니트릴,2-[메톡시(4-페녹시페닐)메틸렌]- 프로판디니트릴,2-[히드록시(4-페녹시페닐)메틸렌]- 8-BOC-3,8-DIAZA-BICYCLO[3.2.1]옥탄 tert-부틸2-옥소-6-아자스피로[3.5]노난-6-카르복실레이트 1-옥사-7-아자스피로[4.5]데칸-7-카르복실산,3-옥소-,1,1-디메틸에틸에스테르 1-Boc-3-메틸-3-하이드록시… N-BOC-3-메틸렌-피페리딘 3-(2-에톡시카보닐-아세틸)-피페리딘-1-카복실산tert-부틸에스테르 1-BOC-4-(4-브로모-벤조일)-피페리딘 1-BOC-4-(4-클로로-벤조일)-피페리딘 tert-부틸4-(4-플루오로벤졸)피페리딘-1-카르복실레이트 4-아세틸-피페리딘-1-카르복실산TERT-부틸에스테르 4-(2-에톡시카보닐-아세틸)-피페리딘-1-카복실산tert-부틸에스테르