1-Fluoro-3-iodo-5-nitrobenzene

1-Fluoro-3-iodo-5-nitrobenzene Suppliers list

Company Name:	Shanghai Harvest Chemical Industrial Co., Ltd. Gold
Tel:	15721252604 17321035817
Email:	sales@harvest-chem.com

Company Name:	Meryer (Shanghai) Chemical Technology Co., Ltd.
Tel:	4006356688 18621169109
Email:	market03@meryer.com

Company Name:	TCI (Shanghai) Development Co., Ltd.
Tel:	021-67121386
Email:	Sales-CN@TCIchemicals.com

1-Fluoro-3-iodo-5-nitrobenzene manufacturers

1-Fluoro-3-iodo-5-nitrobenzene Basic information

Product Name:	1-Fluoro-3-iodo-5-nitrobenzene
Synonyms:	BENZENE, 1-FLUORO-3-IODO-5-NITRO-;3-NITRO-5-FLUORO-IODO-BENZENE;3-FLUORO-5-IODONITROBENZENE;1-Fluoro-3-iodo-5-nitrobenzene,98%;3-Fluoro-5-iodonitrobenzen;1-Fluoro-3-iodo-5-nitrobenzene>;1-Fluoro-3-iodo-5-nitrobenzene , 97%,;1-Fluoro-3-iodo-5-nitrobenzene
CAS:	3819-88-3
MF:	C6H3FINO2
MW:	267
EINECS:
Product Categories:	Aryl Fluorinated Building Blocks;Building Blocks;Chemical Synthesis;Fluorinated Building Blocks;Nitro Compounds;Nitrogen Compounds;Organic Building Blocks;Organic Fluorinated Building Blocks;Other Fluorinated Organic Building Blocks;Nitro Compounds;Nitrogen Compounds;Organic Building Blocks;C6
Mol File:	3819-88-3.mol

1-Fluoro-3-iodo-5-nitrobenzene Chemical Properties

Melting point	77-79 °C (lit.)
Boiling point	277.7±20.0 °C(Predicted)
density	2.093±0.06 g/cm3(Predicted)
storage temp.	Keep in dark place,Inert atmosphere,Room temperature
solubility	soluble in Methanol
form	Powder and/or Chunks
color	Yellow to khaki or brown
Sensitive	Light Sensitive
InChI	InChI=1S/C6H3FINO2/c7-4-1-5(8)3-6(2-4)9(10)11/h1-3H
InChIKey	MXPYCSFCKXSPAB-UHFFFAOYSA-N
SMILES	C1(F)=CC([N+]([O-])=O)=CC(I)=C1

Safety Information

MSDS Information

Provider	Language
ACROS	English
SigmaAldrich	English

1-Fluoro-3-iodo-5-nitrobenzene Usage And Synthesis

Chemical Properties	yellow crystalline powder and chunks
Uses	1-Fluoro-3-iodo-5-nitrobenzene may be used in chemical synthesis.
Synthesis	394-01-4 3819-88-3 In a Schlenk reaction tube equipped with a magnetic stirrer, 6.7 mg of palladium trifluoroacetate (Pd(TFA)2), 28.6 mg of cuprous oxide (Cu2O), 6.4 mg of potassium phosphate (K3PO4), 37 mg of 4-fluoro-2-nitrobenzoic acid, 36 mg of sodium iodide (NaI) and 194 mg of bismuth ammonium nitrate hydrate (Bi(NO3)3- 5H2O). The reaction mixture was heated to 170 °C under oxygen atmosphere with continuous stirring for 20 hours. Upon completion of the reaction, the reaction was quenched by the addition of an appropriate amount of distilled water, followed by extraction with ethyl acetate (10 mL each time) three times and combining the organic phases. The combined organic phases were concentrated to give 29.4 mg of 1-fluoro-3-iodo-5-nitrobenzene in 55% yield.
References	[1] Patent: CN107513020, 2017, A. Location in patent: Paragraph 0057-0058

1-Fluoro-3-iodo-5-nitrobenzene Preparation Products And Raw materials

Raw materials	4-Fluoro-2-nitrobenzoic acid-->Potassium phosphate tribasic-->Palladium(II) trifluoroacetate-->Dimethyl sulfoxide-->Cuprous oxide-->Oxygen-->Sodium iodide-->Bismuth nitrate pentahydrate
Preparation Products	2-Iodo-3-fluoronitrobenzene-->5-Amino-3-fluorobenzonitrile-->1-(3-Fluoro-5-nitrophenyl)ethanone

Tag:1-Fluoro-3-iodo-5-nitrobenzene(3819-88-3) Related Product Information

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