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1-Acetoxy-1-cyanoethylene

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1-Acetoxy-1-cyanoethylene Basic information
Product Name:1-Acetoxy-1-cyanoethylene
Synonyms:1-Cyanovinyl ester of acetic acid;1-Kyanvinylester kyseliny octove;1-kyanvinylesterkyselinyoctove;2-(acetyloxy)-2-propenenitril;2-(acetyloxy)-2-propenenitrile;2-hydroxy-acrylonitrilacetate;2-hydroxy-acrylonitrilacetate(ester);2-Hydroxyacrylonitrile acetate
CAS:3061-65-2
MF:C5H5NO2
MW:111.1
EINECS:221-303-6
Product Categories:Nitrogen Compounds;Organic Building Blocks;Building Blocks;C1 to C5;Chemical Synthesis;Cyanides/Nitriles
Mol File:3061-65-2.mol
1-Acetoxy-1-cyanoethylene Structure
1-Acetoxy-1-cyanoethylene Chemical Properties
Boiling point 80-82 °C30 mm Hg(lit.)
density 1.061 g/mL at 20 °C(lit.)
vapor pressure 30 mm Hg ( 80 °C)
refractive index n20/D 1.426(lit.)
Fp 147 °F
storage temp. Sealed in dry,2-8°C
solubility sol most organic solvents other than pure hydrocarbons.
form clear liquid
color Colorless to Light yellow
BRN 1751158
CAS DataBase Reference3061-65-2(CAS DataBase Reference)
Safety Information
Hazard Codes T
Risk Statements 23/24/25-41-37/38
Safety Statements 36/37/39-45-26
RIDADR UN 3276 6.1/PG 2
WGK Germany 3
RTECS AG4550000
HS Code 2926.90.5050
HazardClass 6.1(a)
PackingGroup II
Toxicityskn-rbt 10 mg/24H open MLD AIHAAP 23,95,62
MSDS Information
ProviderLanguage
SigmaAldrich English
1-Acetoxy-1-cyanoethylene Usage And Synthesis
Reactivity Profile 1-cyanovinyl acetate is a ketene equivalent for use in the Diels-Alder reaction; undergoes other cycloaddition reactions; reacts with nucleophiles and radicals[1].
Safety ProfilePoison by inhalation, ingestion, andskin contact. A skin irritant. Whenheated to decomposition it emits toxic fumes of NOx andCN-.
storage Handling, Storage, and Precautions: highly toxic; use only in a fume hood. Reagent can be absorbed through the skin. Always wear gloves when handling this reagent.
References 1. Ranganathan, S.; Ranganathan, D.; Mehrotra, A. K. S 1977, 289.
2. Brown, D. S.; Paquette, L. A. JOC 1992, 57, 4512.
3. Nowak, R. M. JOC 1963, 28, 1182.
1-Acetoxy-1-cyanoethylene Preparation Products And Raw materials
Tag:1-Acetoxy-1-cyanoethylene(3061-65-2) Related Product Information
Butyl acetate Cyanomethyl formate 1-Acetoxy-1-cyanoethylene 2-Methoxypropene 2-Ethoxypropene VINYL FORMATE Vinyl acetate Glycolonitrile Methoxyacetonitrile Methoxyethene Ethyl vinyl ether Isopropenyl acetate Ammonium acetate Acrylonitrile