trans-2-Aminocyclopentanol hydrochloride

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trans-2-Aminocyclopentanol hydrochloride manufacturers

trans-2-Aminocyclopentanol hydrochloride Basic information
Uses
Product Name:trans-2-Aminocyclopentanol hydrochloride
Synonyms:TRANS-(-)-2-AMINOCYCLOPENTANOL HYDROCHLORIDE;TRANS-2-AMINOCYCLOPENTANOL HYDROCHLORIDE;TRANS-(1R,2R)-2-AMINO-CYCLOPENTANOL HCL;Cyclopentanol, 2-amino-, hydrochloride (1:1), (1R,2R)-;Trans-(-)-2-aminocyclopentanolHCl;trans-(1R,2R)-2-AMinocyclopentanol hydrochloride;(1R,2R)-trans-2-Aminocyclopentanol hydrochloride, 98%, ee: 99%;[1R,2R]-trans-2-Aminocyclopentanol hydrochloride
CAS:68327-11-7
MF:C5H12ClNO
MW:137.61
EINECS:1312995-182-4
Product Categories:Alcohols and Derivatives;68327-11-7
Mol File:68327-11-7.mol
trans-2-Aminocyclopentanol hydrochloride Structure
trans-2-Aminocyclopentanol hydrochloride Chemical Properties
Melting point 191-196 °C(lit.)
storage temp. under inert gas (nitrogen or Argon) at 2-8°C
form powder to crystal
color White to Light yellow to Light orange
BRN 4143621
InChIInChI=1/C5H11NO.ClH/c6-4-2-1-3-5(4)7;/h4-5,7H,1-3,6H2;1H/t4-,5-;/s3
InChIKeyZFSXKSSWYSZPGQ-TXRIQCMBNA-N
SMILES[C@@H]1(O)CCC[C@H]1N.[H]Cl |&1:0,5,r|
CAS DataBase Reference68327-11-7(CAS DataBase Reference)
Safety Information
WGK Germany 3
HS Code 29221990
Storage Class11 - Combustible Solids
MSDS Information
ProviderLanguage
SigmaAldrich English
trans-2-Aminocyclopentanol hydrochloride Usage And Synthesis
Uses(1R,2R)-2-Aminocyclopentanol hydrochloride is a useful research chemical.
Synthesis
Carbamic acid, N-[(1R,2R)-2-hydroxycyclopentyl]-, phenylmethyl ester

672310-36-0

trans-2-Aminocyclopentanol hydrochloride

68327-11-7

To a 100 mL autoclave was added 15 g (70.7 mmol) of (R,R)-2-benzyloxycarbonylaminocyclopentanol and 0.3 g of 5% palladium-carbon catalyst, and 45 mL of degassed methanol under nitrogen protection. The reaction mixture was stirred under 2 MPa hydrogen pressure at 50 °C for 3 hours. Upon completion of the reaction, the palladium-carbon catalyst was removed by diatomaceous earth filtration. Concentrated hydrochloric acid was slowly added to the filtrate to adjust the pH to 3. Subsequently, the aqueous phase was concentrated to afford 7.9 g of trans-(-)-2-aminocyclopentanol hydrochloride in 79.2% yield.

References[1] Patent: EP1398310, 2004, A1. Location in patent: Page 17
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