tert-Butyl N-[(5-formylthiophen-2-yl)methyl]carbamate synthesis
- Product Name:tert-Butyl N-[(5-formylthiophen-2-yl)methyl]carbamate
- CAS Number:1314538-74-3
- Molecular formula:C11H15NO3S
- Molecular Weight:241.31
24424-99-5
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Yield:-
Steps:
Multi-step reaction with 3 steps
1.1: potassium hexamethylsilazane / tetrahydrofuran / 2.25 h / -78 - 20 °C
1.2: 1 h / 0 °C
1.3: 0 - 20 °C
2.1: potassium hydrogen bifluoride / methanol; water / 0 - 20 °C
3.1: palladium diacetate; potassium carbonate; XPhos / water; toluene / 22 h / 85 °C / Inert atmosphere
References:
Molander, Gary A.;Shin, Inji [Organic Letters,2011,vol. 13,# 15,p. 3956 - 3959]
7283-96-7
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![Potassium {[(tert-butoxycarbonyl)amino]methyl}trifluoroborate](/CAS/GIF/1314538-55-0.gif)
1314538-55-0
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