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18162-48-6872-50-4Methylene ChloridenaphthaleneTHFTitanium Dioxide
ChemicalBook CAS DataBase List Methyl 2-((4-butyl-5-((2'-cyano-[1,1'-biphenyl]-4-yl)methyl)-2-methyl-6-oxopyrimidin-1(6H)-yl)methyl)thiophene-3-carboxylate
172292-52-3

Methyl 2-((4-butyl-5-((2'-cyano-[1,1'-biphenyl]-4-yl)methyl)-2-methyl-6-oxopyrimidin-1(6H)-yl)methyl)thiophene-3-carboxylate synthesis

6synthesis methods
1918-78-1 Synthesis
2-Methyl-thiophene-3-carboxylic acid

1918-78-1
79 suppliers
$9.00/250mg

Methyl 2-((4-butyl-5-((2'-cyano-[1,1'-biphenyl]-4-yl)methyl)-2-methyl-6-oxopyrimidin-1(6H)-yl)methyl)thiophene-3-carboxylate

172292-52-3
18 suppliers
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-

Yield:-

Steps:

Multi-step reaction with 3 steps
1: H2SO4
2: 75 percent / N-bromosuccinimide, α,α'-azoisobutyronitrile / CCl4 / 3 h / 70 °C
3: 1.) NaH, 2.) LiBr

References:

Salimbeni, Aldo;Canevotti, Renato;Paleari, Fabio;Poma, Davide;Caliari, Saturnino;et al. [Journal of Medicinal Chemistry,1995,vol. 38,# 24,p. 4806 - 4820]

53562-51-9 Synthesis
2-Methyl-3-thiophenecarboxylic acid methyl ester

53562-51-9
83 suppliers
$52.00/1g

Methyl 2-((4-butyl-5-((2'-cyano-[1,1'-biphenyl]-4-yl)methyl)-2-methyl-6-oxopyrimidin-1(6H)-yl)methyl)thiophene-3-carboxylate

172292-52-3
18 suppliers
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References
39815-78-6 Synthesis
Methyl 3-oxoheptanoate

39815-78-6
111 suppliers
$91.67/25g

Methyl 2-((4-butyl-5-((2'-cyano-[1,1'-biphenyl]-4-yl)methyl)-2-methyl-6-oxopyrimidin-1(6H)-yl)methyl)thiophene-3-carboxylate

172292-52-3
18 suppliers
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References
4-Bromomethyl-2-cyanobiphenyl

114772-54-2
595 suppliers
$5.00/5g

Methyl 2-((4-butyl-5-((2'-cyano-[1,1'-biphenyl]-4-yl)methyl)-2-methyl-6-oxopyrimidin-1(6H)-yl)methyl)thiophene-3-carboxylate

172292-52-3
18 suppliers
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References
148564-09-4

148564-09-4
1 suppliers
inquiry

Methyl 2-((4-butyl-5-((2'-cyano-[1,1'-biphenyl]-4-yl)methyl)-2-methyl-6-oxopyrimidin-1(6H)-yl)methyl)thiophene-3-carboxylate

172292-52-3
18 suppliers
inquiry

References