2-Ethylaniline synthesis
- Product Name:2-Ethylaniline
- CAS Number:578-54-1
- Molecular formula:C8H11N
- Molecular Weight:121.18
35774-47-1
3 suppliers
inquiry
578-54-1
267 suppliers
$10.00/5g
Yield:578-54-1 90%
Reaction Conditions:
with iron in water at 20;Inert atmosphere;
Steps:
General experimental procedure for reduction of azidoarenes
General procedure: The azido compound (1 mmol) was added to the freshly prepared Fe(0) nanoparticles (3 mmol) in water (5 mL) in the same pot under constant stirring at room temperature under argon atmosphere. After completion of reaction (TLC) the mixture was extracted with ethyl acetate (3 X 10 mL) (all Fe-species remained around stirring bar). Evaporation of solvent and purification by short column chromatography provided the pure product which was properly characterized by spectroscopic (IR, 1H NMR and 13C NMR) data.
References:
Panja, Subir;kundu, Debasish;Ahammed, Sabir;Ranu, Brindaban C. [Tetrahedron Letters,2017,vol. 58,# 35,p. 3457 - 3460] Location in patent:supporting information
120-72-9
666 suppliers
$6.00/25g
496-15-1
444 suppliers
$8.00/10g
578-54-1
267 suppliers
$10.00/5g
1678-91-7
207 suppliers
$36.00/25mL
100-41-4
376 suppliers
$5.00/5 g
1821-38-1
14 suppliers
inquiry
578-54-1
267 suppliers
$10.00/5g
612-22-6
141 suppliers
$14.00/5g
578-54-1
267 suppliers
$10.00/5g
577-59-3
280 suppliers
$6.00/5g
578-54-1
267 suppliers
$10.00/5g