2-Ethylhexyl nitrate synthesis
- Product Name:2-Ethylhexyl nitrate
- CAS Number:27247-96-7
- Molecular formula:C8H17NO3
- Molecular Weight:175.23
104-76-7
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27247-96-7
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Yield:27247-96-7 100%
Reaction Conditions:
with sulfuric acid;nitric acid at 10; for 0.0333333 h;Large scale;
Steps:
2
[0029] A G4 Advanced-Flow reactor from Corning was configured and set up according to the description of Figure 4. A pump for 98% HN03 was set to l .OlKg/min (0.72L/min, 16mol/min), and a pump for 90% H2S04 was set to 3.03Kg/min (1.67L/min, 27.8mol/min), while a pump for alcohol was set to 2.08Kg/min (2.5L/min, 16mol/min), with a the chiller temperature set to 10° C. Samples were collected after the system stabilized (at about 2 minutes). GC analysis showed a full conversion of the starting material, and the yield was 100%. With total internal volume of 1.0L (4 modules), the retention time was (1.0L)/(4.89L/min)*60=12s (or liquid space velocity of 290h_1).
References:
CORNING INCORPORATED;MA, Bing;SHEN, Wei;WANG, Yanhua;ZHANG, Mo WO2015/134703, 2015, A1 Location in patent:Paragraph 0029
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149-57-5
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7425-14-1
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27247-96-7
235 suppliers
$72.00/1l