ChemicalBook CAS DataBase List 1,3-Benzodioxole-5-methanamine, .alpha.-methyl-, (.alpha.S)-

1,3-Benzodioxole-5-methanamine, .alpha.-methyl-, (.alpha.S)- synthesis

2synthesis methods

Product Name:1,3-Benzodioxole-5-methanamine, .alpha.-methyl-, (.alpha.S)-
CAS Number:210488-52-1
Molecular formula:C9H11NO2
Molecular Weight:165.19

3162-29-6 Synthesis

3162-29-6
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1,3-Benzodioxole-5-methanamine, .alpha.-methyl-, (.alpha.S)-

210488-52-1
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Yield:-

Steps:

Multi-step reaction with 3 steps
1: titanium(IV) tetraethanolate / tetrahydrofuran / 30 h / 20 °C / Reflux
2: L-Selectride / tetrahydrofuran / 1.5 h / -50 °C / Inert atmosphere
3: thionyl chloride / methanol / 1.25 h / 0 - 20 °C

References:

WO2016/30443,2016,A1

1-Butanol, 2-[[(1S)-1-(1,3-benzodioxol-5-yl)ethyl]amino]-3-methyl-, (2S)-

1010385-15-5
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210488-52-1
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References

1,3-Benzodioxole-5-methanamine, .alpha.-methyl-, (.alpha.S)- Related Search:

1,3-Benzodioxole-5-methanamine, .alpha.-methyl-, (.alpha.R)-

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