3-(2-METHOXY-PHENYL)-PROPIONALDEHYDE synthesis
- Product Name:3-(2-METHOXY-PHENYL)-PROPIONALDEHYDE
- CAS Number:33538-83-9
- Molecular formula:C10H12O2
- Molecular Weight:164.2
1504-74-1
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$7.00/100mg
33538-83-9
38 suppliers
$75.00/100mg
Yield: 54%
Reaction Conditions:
with palladium on activated charcoal in methanol at 20; for 2 h;
Steps:
3-(2-Methoxyphenyl)propanal
The suspension of 2-methoxycinnamaldehyde (1.00 g, 6.17 mmol) and Pd/C (131 mg, 0.20 mmol) werestirred in MeOH (12 mL) at room temperature for 2 h. The reaction mixture was filtered on celite with dichloromethane. The mixture solvent was evaporated under reduced pressure, and the residue was purifiedby column chromatography with hexane/ethyl acetate (3/1, v/v) to obtain 3-(2-methoxyphenyl)propanal.
References:
Lee, Ju-Hyeon;Shin, Sang Chul;Seo, Seon Hee;Seo, Young Ho;Jeong, Nakcheol;Kim, Chan-Wha;Kim, Eunice EunKyeong;Keum, Gyochang [Bioorganic and Medicinal Chemistry Letters,2017,vol. 27,# 2,p. 237 - 241] Location in patent:supporting information
10493-37-5
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$27.00/100mg
33538-83-9
38 suppliers
$75.00/100mg
5720-06-9
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$5.00/1g
107-18-6
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$24.60/100ml
33538-83-9
38 suppliers
$75.00/100mg
79-37-8
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$17.67/10gm:
10493-37-5
63 suppliers
$27.00/100mg
33538-83-9
38 suppliers
$75.00/100mg
64-18-6
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$22.13/250ML
612-15-7
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$50.50/1g
33538-83-9
38 suppliers
$75.00/100mg