1,1,2,2,3,3,4,4,4-Nonafluoro-N-(2-methoxyethyl)-1-butanesulfonamide synthesis
1synthesis methods
- Product Name:1,1,2,2,3,3,4,4,4-Nonafluoro-N-(2-methoxyethyl)-1-butanesulfonamide
- CAS Number:40630-68-0
- Molecular formula:C7H8F9NO3S
- Molecular Weight:357.19
Yield:40630-68-0 47%
Reaction Conditions:
Stage #1: Nonafluorobutanesulfonyl fluoride;2-methoxyethylaminewith triethylamine in acetonitrile at 0 - 20; for 17 h;
Stage #2: in acetonitrile; for 3 h;Heating;Further stages.;
References:
Lehmler, Hans-Joachim;Rama Rao;Nauduri, Dhananjaya;Vargo, John D.;Parkin, Sean [Journal of Fluorine Chemistry,2007,vol. 128,# 6,p. 595 - 607]