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ChemicalBook CAS DataBase List 5'-O-TRITYL-2'-DEOXY-BETA-D-LYXOFURANOSYLTHYMINE
55612-11-8

5'-O-TRITYL-2'-DEOXY-BETA-D-LYXOFURANOSYLTHYMINE synthesis

13synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 4 steps
1: Na
2: 70 percent / NaH / dimethylformamide
3: 63 percent / Rh(PPh3)3Cl, pyridine / aq. ethanol / 5 h / Heating
4: 60 percent / pyridine*HF / dioxane

References:

Xia, Xiaoyang;Wang, Jianying;Hager, Michael W.;Sisti, Nicholas;Liotta, Dennis C. [Tetrahedron Letters,1997,vol. 38,# 7,p. 1111 - 1114]