(2-Amino-4-chloro-phenyl)-carbamic acid tert-butyl ester synthesis
- Product Name:(2-Amino-4-chloro-phenyl)-carbamic acid tert-butyl ester
- CAS Number:579474-49-0
- Molecular formula:C11H15ClN2O2
- Molecular Weight:242.7
24424-99-5
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Yield:-
Steps:
Multi-step reaction with 2 steps
1.1: sodium hydride / N,N-dimethyl-formamide / 0.67 h / 0 - 20 °C
1.2: 15 h / 20 °C
2.1: sodium dithionite; sodium hydrogencarbonate / 1,4-dioxane; water / 0.67 h / 100 °C
References:
Kilchmann, Falco;Marcaida, Maria J.;Kotak, Sachin;Schick, Thomas;Boss, Silvan D.;Awale, Mahendra;G?nczy, Pierre;Reymond, Jean-Louis [Journal of Medicinal Chemistry,2016,vol. 59,# 15,p. 7188 - 7211]
89-63-4
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