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18162-48-6872-50-4Methylene ChloridenaphthaleneTHFTitanium Dioxide
ChemicalBook CAS DataBase List (2S,2'S)-(-)-2-HYDROXYMETHYL-1-[(1-METHYLPYRROLIDIN-2-YL)-METHYL]-PYRROLIDINE
66283-23-6

(2S,2'S)-(-)-2-HYDROXYMETHYL-1-[(1-METHYLPYRROLIDIN-2-YL)-METHYL]-PYRROLIDINE synthesis

3synthesis methods
Preparative Method of (2S,2′S)-2-Hydroxymethyl-1-[(1-methylpyrrolidin-2-yl)methyl]pyrrolidine: reduction of N-[N(-benzyloxycarbonyl)prolyl]proline methyl ester with Lithium Aluminum Hydride affords the title reagent in 81% yield.
L-Proline, 1-[1-[(phenylmethoxy)carbonyl]-L-prolyl]-, methyl ester

17708-83-7
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(2S,2'S)-(-)-2-HYDROXYMETHYL-1-[(1-METHYLPYRROLIDIN-2-YL)-METHYL]-PYRROLIDINE

66283-23-6
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Yield:66283-23-6 81%

Reaction Conditions:

with lithium aluminium tetrahydride in tetrahydrofuran; for 3 h;Heating;

References:

Mukaiyama, Teruaki [Tetrahedron,1981,vol. 37,# 23,p. 4111 - 4119]

147-85-3 Synthesis
L-Proline

147-85-3
1064 suppliers
$6.00/25g

(2S,2'S)-(-)-2-HYDROXYMETHYL-1-[(1-METHYLPYRROLIDIN-2-YL)-METHYL]-PYRROLIDINE

66283-23-6
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References
N-Benzyloxycarbonyl-L-proline

1148-11-4
463 suppliers
$6.00/10g

(2S,2'S)-(-)-2-HYDROXYMETHYL-1-[(1-METHYLPYRROLIDIN-2-YL)-METHYL]-PYRROLIDINE

66283-23-6
14 suppliers
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References

(2S,2'S)-(-)-2-HYDROXYMETHYL-1-[(1-METHYLPYRROLIDIN-2-YL)-METHYL]-PYRROLIDINE Related Search:

Z-PRO-PRO-OH H-GLY-PRO-PRO-OH H-GLY-PRO-HYP-OH