Boronic acid, [4-chloro-1-[tris(1-methylethyl)silyl]-1H-pyrrolo[2,3-b]pyridin-5-yl]- (9CI) synthesis
- Product Name:Boronic acid, [4-chloro-1-[tris(1-methylethyl)silyl]-1H-pyrrolo[2,3-b]pyridin-5-yl]- (9CI)
- CAS Number:685513-99-9
- Molecular formula:C16H26BClN2O2Si
- Molecular Weight:352.74
![1H-Pyrrolo[2,3-b]pyridine, 4-chloro-1-[tris(1-methylethyl)silyl]-](/CAS/GIF/651744-48-8.gif)
651744-48-8
76 suppliers
$225.00/1g
685513-99-9
15 suppliers
$501.20/5MG
Yield:685513-99-9 47%
Reaction Conditions:
Stage #1: 4-chloro-1-triisopropylsilanyl-1H-pyrrolo[2,3-b]pyridinewith sec.-butyllithium in tetrahydrofuran;cyclohexane at -78; for 0.5 h;
Stage #2: with Triisopropyl borate in tetrahydrofuran;cyclohexane at -78; for 0.416667 h;Further stages.;
References:
L'Heureux, Alexandre;Thibault, Carl;Ruel, Réjean [Tetrahedron Letters,2004,vol. 45,# 11,p. 2317 - 2319]
13154-24-0
418 suppliers
$20.00/10g
685513-99-9
15 suppliers
$501.20/5MG
55052-28-3
456 suppliers
$6.00/1g
685513-99-9
15 suppliers
$501.20/5MG