ChemicalBook CAS DataBase List (2S)-2-[3-({[(9H-fluoren-9-yl)methoxy]carbonyl}amino)propanamido]propanoic acid

(2S)-2-[3-({[(9H-fluoren-9-yl)methoxy]carbonyl}amino)propanamido]propanoic acid synthesis

2synthesis methods

Product Name:(2S)-2-[3-({[(9H-fluoren-9-yl)methoxy]carbonyl}amino)propanamido]propanoic acid
CAS Number:850324-83-3
Molecular formula:C21H22N2O5
Molecular Weight:382.4098

35737-10-1 Synthesis

35737-10-1
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(2S)-2-[3-({[(9H-fluoren-9-yl)methoxy]carbonyl}amino)propanamido]propanoic acid

850324-83-3
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Yield:-

Steps:

Multi-step reaction with 2 steps
1: (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 2 h
2: trifluoroacetic acid / chloroform / 23 h

References:

Marty, Roman;Nigon, Robin;Leite, Deborah;Frauenrath, Holger [Journal of the American Chemical Society,2014,vol. 136,# 10,p. 3919 - 3927]

Ethanamine, N-[(3,5-dichlorophenyl)methylene]-2,2-diethoxy-

1000210-73-0
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850324-83-3
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References

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