CarbaMic acid, N-5-isothiazolyl-,1,1- diMethylethyl ester synthesis
- Product Name:CarbaMic acid, N-5-isothiazolyl-,1,1- diMethylethyl ester
- CAS Number:887475-44-7
- Molecular formula:C8H12N2O2S
- Molecular Weight:200.26
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Yield: 97%
Reaction Conditions:
with diphenyl phosphoryl azide;triethylamine at 100; for 4 h;Curtius Rearrangement;
References:
Pei, Zhonghua;Mendonca, Rohan;Gazzard, Lewis;Pastor, Richard;Goon, Leanne;Gustafson, Amy;Vanderporten, Erica;Hatzivassiliou, Georgia;Dement, Kevin;Cass, Robert;Yuen, Po-Wai;Zhang, Yamin;Wu, Guosheng;Lin, Xingyu;Liu, Yichin;Sellers, Benjamin D. [ACS Medicinal Chemistry Letters,2018,vol. 9,# 5,p. 417 - 421] Location in patent:supporting information