3-quinolinecarboxylic acid, 1-(6-amino-3,5-difluoro-2-pyridinyl)-8-chloro-6,7-difluoro-1,4-dihydro-4-oxo-, ethyl ester synthesis
- Product Name:3-quinolinecarboxylic acid, 1-(6-amino-3,5-difluoro-2-pyridinyl)-8-chloro-6,7-difluoro-1,4-dihydro-4-oxo-, ethyl ester
- CAS Number:906088-96-8
- Molecular formula:C17H11F4N3O3
- Molecular Weight:381.28
101799-75-1
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Yield:-
Steps:
Multi-step reaction with 2 steps
1: 1-methyl-pyrrolidin-2-one / acetonitrile / 1 h / Large scale
2: 1-methyl-pyrrolidin-2-one; lithium chloride; 1,8-diazabicyclo[5.4.0]undec-7-ene / 3.67 h / 23 - 35 °C
References:
Barnes, David M.;Christesen, Alan C.;Engstrom, Kenneth M.;Haight, Anthony R.;Hsu, Margaret C.;Lee, Elaine C.;Peterson, Matthew J.;Plata, Daniel J.;Raje, Prasad S.;Stoner, Eric J.;Tedrow, Jason S.;Wagaw, Seble [Organic Process Research and Development,2006,vol. 10,# 4,p. 803 - 807]
98349-24-7
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$6.00/250mg
906088-96-8
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446-17-3
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88419-56-1
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$10.00/1g
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