Ethyl 7-bromo-1-oxo-3,4-dihydro-2H-naphthalene-2-carboxylate synthesis
- Product Name:Ethyl 7-bromo-1-oxo-3,4-dihydro-2H-naphthalene-2-carboxylate
- CAS Number:914262-72-9
- Molecular formula:C13H13BrO3
- Molecular Weight:297.14
32281-97-3
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105-58-8
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Yield:914262-72-9 83%
Reaction Conditions:
Stage #1: Diethyl carbonatewith sodium hydride in benzene at 65;
Stage #2: 7-bromo-3,4-dihydro-2H-naphthalen-1-one in benzene; for 3 h;Heating;
References:
Chackal-Catoen, Sarah;Miao, Yi;Wilson, W. David;Wenzler, Tanja;Brun, Reto;Boykin, David W. [Bioorganic and Medicinal Chemistry,2006,vol. 14,# 22,p. 7434 - 7445]
35656-89-4
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6340-79-0
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$5.00/250mg
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181765-86-6
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