Ethyl 5-chloro-1-benzothiophene-2-carboxylate synthesis
- Product Name:Ethyl 5-chloro-1-benzothiophene-2-carboxylate
- CAS Number:13771-67-0
- Molecular formula:C11H9ClO2S
- Molecular Weight:240.71
20532-33-6
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Yield:13771-67-0 30%
Reaction Conditions:
with phosphovanadomolybdic acid;oxygen;palladium diacetate;N-acetylglycine in N,N-dimethyl-formamide at 120; under 760.051 Torr; for 24 h;Sealed tube;
References:
Huang, Qiufeng;Ke, Shaojia;Qiu, Lin;Zhang, Xiaofeng;Lin, Shen [ChemCatChem,2014,vol. 6,# 6,p. 1531 - 1534]