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ChemicalBook CAS DataBase List FMOC-L-BETA-HOMOLEUCINE
193887-44-4

FMOC-L-BETA-HOMOLEUCINE synthesis

4synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1: 1.) i-BuOCOCl, NMM / 1.) THF, -20 deg C, 20 min, 2.) THF, Et2O, -5 deg C, 4 h
2: 66 percent / CF3COOAg, Et3N / tetrahydrofuran; H2O

References:

Guichard, Gilles;Abele, Stefan;Seebach, Dieter [Helvetica Chimica Acta,1998,vol. 81,# 2,p. 187 - 206]

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