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ChemicalBook CAS DataBase List N-VANILLYLOCTANAMIDE
58493-47-3

N-VANILLYLOCTANAMIDE synthesis

5synthesis methods
-

Yield:58493-47-3 94.1%

Reaction Conditions:

Stage #1: vanillylamine hydrochloridewith sodium hydrogencarbonate in water at 20; for 0.5 h;
Stage #2: n-octanoic acid chloride in chloroform;water at 20; for 0.5 h;

References:

Wang, Bo;Yang, Fan;Shan, Yi-Fan;Qiu, Wen-Wei;Tang, Jie [Tetrahedron,2009,vol. 65,# 27,p. 5409 - 5412] Location in patent:supporting information; experimental part

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