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ChemicalBook CAS DataBase List POTASSIUM (4-METHOXYCARBONYLPHENYL)TRIFLUOROBORATE
705254-34-8

POTASSIUM (4-METHOXYCARBONYLPHENYL)TRIFLUOROBORATE synthesis

6synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1: tetrahydroxydiboron; (chloro(2-dicyclohexylphosphino-2′,4′,6′-triisopropyl-1,1′-biphenyl)[2-(2′-amino-1,1′-biphenyl)]palladium(II)); potassium acetate; XPhos / ethanol / 3 h / 80 °C / Inert atmosphere
2: potassium hydrogenfluoride / methanol; water / 0.5 h / 0 - 20 °C / Inert atmosphere

References:

Molander, Gary A.;Trice, Sarah L. J.;Kennedy, Steven M.;Dreher, Spencer D.;Tudge, Matthew T. [Journal of the American Chemical Society,2012,vol. 134,# 28,p. 11667 - 11673]

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