PYRIDINE-2,3,6-TRIAMINE synthesis
- Product Name:PYRIDINE-2,3,6-TRIAMINE
- CAS Number:4318-79-0
- Molecular formula:C5H8N4
- Molecular Weight:124.14
3346-63-2
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$113.00/100mg
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Yield:4318-79-0 78%
Reaction Conditions:
with palladium 10% on activated carbon;hydrogen in methanol at 20; for 2 h;
Steps:
1.3 Step 3: Synthesis of pyridine-2, 3, 6-triamine (5)
To a solution of 4 (1.6 g, 10.38 mmol) in methanol (20 mL) was added 10% Pd/C (160 mg) and the resulting reaction mixture was stirred under hydrogen atmosphere at room temperature for 2 hours. After completion of reaction, the reaction mixture was filtered over a pad of cealite and washed with methanol. Filtrate was evaporated under reduced pressure to give the desired product 5 (1 g, 78%) as a purple color solid that was pure enough to take ahead for next step
References:
WO2020/120576,2020,A1 Location in patent:Page/Page column 34-35
89323-10-4
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94-78-0
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27048-04-0
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13615-50-4
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