(PYRROLIDIN-1-YLCARBONOTHIOYL)THIO]ACETIC ACID synthesis
- Product Name:(PYRROLIDIN-1-YLCARBONOTHIOYL)THIO]ACETIC ACID
- CAS Number:20069-28-7
- Molecular formula:C7H11NO2S2
- Molecular Weight:205.3
109-01-3
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75-15-0
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79-11-8
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Yield:20069-28-7 123.73 g
Reaction Conditions:
Stage #1: 1-methyl-piperazine;carbon disulfidewith potassium hydroxide in ethanol;water at 20; for 1 h;Cooling with ice;
Stage #2: chloroacetic acidwith sodium carbonate in ethanol;water; for 0.12 h;
Stage #3: with hydrazine hydrate;potassium hydroxide for 1 h;Reflux;
References:
Knak, Stefanie;Pfeiffer, Wolf-Diethard;Dollinger, Horst;Langer, Peter [Journal of Heterocyclic Chemistry,2015,vol. 52,# 2,p. 450 - 462]
123-75-1
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75-15-0
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79-11-8
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$27.00/25g
20069-28-7
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123-75-1
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$10.00/5g
75-15-0
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$40.00/100g
3926-62-3
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20069-28-7
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