3-Hydroxy-2-iodo-6-methylpyridine
- CAS No.
- 23003-30-7
- Chemical Name:
- 3-Hydroxy-2-iodo-6-methylpyridine
- Synonyms
- 3-Hydroxy-2-iodo-6-;6-IODO-2-PICOLIN-5-OL;6-Iodo-2-picolin-5-ol,97%;6-IODO-2-PICOLIN-5-OL 97%;2-IODO-3-HYDROXY-6-PICOLINE;2-IODO-6-METHYL-3-PYRIDINOL;3-Pyridinol, 2-iodo-6-methyl-;2-IODO-6-METHYL-3-HYDROXYPYRIDINE;3-HYDROXY-2-IODO-6-METHYLPYRIDINE;2-Iodo-3-hydroxy-6-methylpyridine
- CBNumber:
- CB6108522
- Molecular Formula:
- C6H6INO
- Molecular Weight:
- 235.02
- MDL Number:
- MFCD00006246
- MOL File:
- 23003-30-7.mol
- MSDS File:
- SDS
| Melting point | 197-199 °C (lit.) |
|---|---|
| Boiling point | 292.0±35.0 °C(Predicted) |
| Density | 1.8615 (estimate) |
| storage temp. | Keep in dark place,Sealed in dry,Room Temperature |
| pka | 5.46±0.10(Predicted) |
| Appearance | White to light brown Solid |
| InChI | InChI=1S/C6H6INO/c1-4-2-3-5(9)6(7)8-4/h2-3,9H,1H3 |
| InChIKey | HRZOWBGCOJWHDY-UHFFFAOYSA-N |
| SMILES | C1(I)=NC(C)=CC=C1O |
| CAS DataBase Reference | 23003-30-7(CAS DataBase Reference) |
| UNSPSC Code | 12352100 |
| NACRES | NA.22 |
SAFETY
Risk and Safety Statements
| Symbol(GHS) |  GHS07 |
|---|---|
| Signal word | Warning |
| Hazard statements | H315-H319-H335 |
| Precautionary statements | P261-P264-P271-P280-P302+P352-P305+P351+P338 |
| Hazard Codes | Xi |
| Risk Statements | 36/37/38 |
| Safety Statements | 26-37/39-24/25 |
| WGK Germany | 3 |
| HS Code | 29333999 |
3-Hydroxy-2-iodo-6-methylpyridine price More Price(33)
| Manufacturer | Product number | Product description | CAS number | Packaging | Price | Updated | Buy |
|---|---|---|---|---|---|---|---|
| Sigma-Aldrich | 119024 | 3-Hydroxy-2-iodo-6-methylpyridine 97% | 23003-30-7 | 1g | $79.5 | 2023-06-20 | Buy |
| Usbiological | 279707 | 3-Hydroxy-2-iodo-6-methylpyridine | 23003-30-7 | 1g | $345 | 2021-12-16 | Buy |
| TRC | H943618 | 3-Hydroxy-2-iodo-6-methylpyridine | 23003-30-7 | 500mg | $75 | 2021-12-16 | Buy |
| TRC | H943618 | 3-Hydroxy-2-iodo-6-methylpyridine | 23003-30-7 | 50mg | $45 | 2021-12-16 | Buy |
| Oakwood | 076967 | 3-Hydroxy-2-iodo-6-methylpyridine 97% | 23003-30-7 | 250mg | $14 | 2021-12-16 | Buy |
3-Hydroxy-2-iodo-6-methylpyridine Chemical Properties,Uses,Production
Chemical Properties
Light yellow to yellow powder
Synthesis
1121-78-4
23003-30-7
Step A: 6-Methylpyridin-3-ol (0.5 g, 4.58 mmol) was dissolved in aqueous sodium hydroxide solution (4.5 mL, 1 M, 4.5 mmol). Iodine (1.28 g, 5.2 mmol) was added to this solution and the reaction mixture was stirred overnight at room temperature. After completion of the reaction, it was neutralized with aqueous hydrochloric acid (2 M) to pH ≈ 7. A white precipitate precipitated from the reaction system and the product was collected by filtration. The solid product was washed with deionized water and dried to give 2-iodo-6-methylpyridin-3-ol (0.8 g, 50% yield). Mass spectral analysis showed m/z 236.0 [M + H]+.
References
[1] Bioorganic and Medicinal Chemistry Letters, 1998, vol. 8, # 16, p. 2117 - 2122
[2] Patent: US9617268, 2017, B2. Location in patent: Page/Page column 400; 401
[3] Patent: EP1477186, 2004, A1. Location in patent: Page/Page column 35; 36
[4] Patent: EP1357111, 2003, A1. Location in patent: Page/Page column 54
[5] Tetrahedron, 2007, vol. 63, # 13, p. 2787 - 2797
3-Hydroxy-2-iodo-6-methylpyridine Preparation Products And Raw materials
| Supplier | Tel | Country | ProdList | Advantage | |
|---|---|---|---|---|---|
| Frapp's ChemicalNFTZ Co., Ltd. | +86 (576) 8169-6106 | sales@frappschem.com | China | 880 | 50 |
| ATK CHEMICAL COMPANY LIMITED | +undefined-21-51877795 | ivan@atkchemical.com | China | 33024 | 60 |
| career henan chemical co | +86-0371-86658258 +8613203830695 | sales@coreychem.com | China | 29852 | 58 |
| Shenzhen Nexconn Pharmatechs Ltd | +86-755-89396905 +86-15013857715 | admin@nexconn.com | China | 10406 | 58 |
| Nanjing Dolon Biotechnology Co.,Ltd. | 18905173768 | 52513593@qq.com | CHINA | 2972 | 58 |
| Hubei Jusheng Technology Co.,Ltd. | 18871490254 | linda@hubeijusheng.com | CHINA | 28172 | 58 |
| Alchem Pharmtech,Inc. | 8485655694 | sales@alchempharmtech.com | United States | 63687 | 58 |
| Zhengzhou Alfa Chemical Co.,Ltd | +8618530059196 | sale04@alfachem.cn | China | 12079 | 58 |
| SIMAGCHEM CORP | +86-5922680277 +86-13806087780 | sale@simagchem.com | China | 17346 | 58 |
| ANHUI WITOP BIOTECH CO., LTD | +8615255079626 | eric@witopchemical.com | China | 23541 | 58 |
View Lastest Price from 3-Hydroxy-2-iodo-6-methylpyridine manufacturers
| Image | Update time | Product | Price | Min. Order | Purity | Supply Ability | Manufacturer | |
|---|---|---|---|---|---|---|---|---|
 |
2021-09-25 | 3-Hydroxy-2-iodo-6-methylpyridine
23003-30-7
|
US $1.10 / g | 1g | 99.00% | 100 Tons Min | Dideu Industries Group Limited | |
 |
2019-07-06 | 3-Hydroxy-2-iodo-6-methylpyridine
23003-30-7
|
US $3.00 / KG | 1KG | 99% | 100kg | Career Henan Chemical Co |
-
- 3-Hydroxy-2-iodo-6-methylpyridine
23003-30-7
- US $1.10 / g
- 99.00%
- Dideu Industries Group Limited
-
- 3-Hydroxy-2-iodo-6-methylpyridine
23003-30-7
- US $3.00 / KG
- 99%
- Career Henan Chemical Co
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