4-n-Hexyloxybromobenzene
- CAS No.
- 30752-19-3
- Chemical Name:
- 4-n-Hexyloxybromobenzene
- Synonyms
- TIMTEC-BB SBB008641;P-HEXYLOXYBROMOBENZENE;4-HEXYLOXYBROMOBENZENE;1-bromo-4-hexoxybenzene;P-BROMO(HEXYLOXY)BENZENE;1-(4-BROMOPHENOXY)HEXANE;4-n-Hexyloxybromobenzene;1-BROMO-4-HEXYLOXYBENZENE;4-BROMOPHENYL HEXYL ETHER;4-Bromo-(hexyloxy)-benzene
- CBNumber:
- CB6225324
- Molecular Formula:
- C12H17BrO
- Molecular Weight:
- 257.17
- MDL Number:
- MFCD00173753
- MOL File:
- 30752-19-3.mol
- MSDS File:
- SDS
| Boiling point | 154°C/12mmHg(lit.) |
|---|---|
| Density | 1,23 g/cm3 |
| refractive index | 1.5240 |
| Flash point | >110°(230°F) |
| storage temp. | Sealed in dry,Room Temperature |
| form | clear liquid |
| color | Colorless to Light yellow |
| CAS DataBase Reference | 30752-19-3(CAS DataBase Reference) |
| EPA Substance Registry System | p-Bromophenylhexyl ether (30752-19-3) |
SAFETY
Risk and Safety Statements
| Symbol(GHS) |  GHS07 |
|||||||||
|---|---|---|---|---|---|---|---|---|---|---|
| Signal word | Warning | |||||||||
| Hazard statements | H315-H319-H335 | |||||||||
| Precautionary statements | P261-P305+P351+P338 | |||||||||
| TSCA | TSCA listed | |||||||||
| HS Code | 2909303890 | |||||||||
| NFPA 704 |
|
4-n-Hexyloxybromobenzene price More Price(37)
| Manufacturer | Product number | Product description | CAS number | Packaging | Price | Updated | Buy |
|---|---|---|---|---|---|---|---|
| TCI Chemical | B3876 | 1-Bromo-4-hexyloxybenzene >98.0%(GC) | 30752-19-3 | 5g | $43 | 2026-04-30 | Buy |
| TCI Chemical | B3876 | 1-Bromo-4-hexyloxybenzene >98.0%(GC) | 30752-19-3 | 25g | $124 | 2026-04-30 | Buy |
| Apolloscientific | OR21905 | 1-(4-Bromophenoxy)hexane 98% | 30752-19-3 | 1g | $21 | 2026-06-04 | Buy |
| Apolloscientific | OR21905 | 1-(4-Bromophenoxy)hexane 98% | 30752-19-3 | 5g | $24 | 2026-06-04 | Buy |
| Apolloscientific | OR21905 | 1-(4-Bromophenoxy)hexane 98% | 30752-19-3 | 25g | $74 | 2026-06-04 | Buy |
4-n-Hexyloxybromobenzene Chemical Properties, Uses, Production
Synthesis
106-41-2
111-25-1
30752-19-3
Example 3.1 Synthesis of 1-bromo-4-(hexyloxy)benzene: Increase the temperature of the oil bath to 65 °C. In a 500 mL round-bottomed flask fitted with a stirrer, 10 g (57.8 mmol, 1.0 eq.) of 4-bromophenol and 26.36 g (190.7 mmol, 3.3 eq.) of potassium carbonate were added sequentially, followed by 202.3 mL of acetone. The reaction vessel was sealed, a condenser tube was fitted and purged continuously with argon for 10 min. After completion of the purge, 8.9 mL (64 mmol, 1.1 eq.) of bromohexane was slowly added via syringe, and the reaction mixture was stirred under reflux conditions in an oil bath for 24 hours. The progress of the reaction was monitored by thin layer chromatography (silica gel plate, hexane as the unfolding agent) and after confirming the completion of the reaction, the crude reaction mixture was filtered to remove potassium carbonate. Water was added to the filtrate and extracted twice with ether. The ether extracts were combined and dried with magnesium sulfate, followed by filtration to remove the desiccant. The solvent was removed by distillation under reduced pressure and the crude product obtained was purified by silica gel column chromatography (eluent hexane) to give 13.96 g (93.9% yield) of the target product 1-bromo-4-(hexyloxy)benzene as a clear liquid.GC-MS analysis showed the correct molecular ion peaks.1H NMR (500 MHz, CDCl3, internal standard TMS, δ 7.26 ppm): δ 7.355 (m, 2H), 6.770 (m, 2H), 3.912 (t, J = 6.75 Hz, 2H), 1.764 (m, 2H), 1.49-1.40 (m, 2H), 1.37-1.30 (m, 4H), 0.905 (t, J = 7.0 Hz, 3H).
References
[1] Angewandte Chemie - International Edition, 2014, vol. 53, # 12, p. 3168 - 3172
[2] Angew. Chem., 2014, vol. 126, # 12, p. 3232 - 3236,5
[3] European Journal of Organic Chemistry, 2013, # 26, p. 5917 - 5922
[4] Chemistry - A European Journal, 2017, vol. 23, # 17, p. 4149 - 4159
[5] Helvetica Chimica Acta, 2009, vol. 92, # 6, p. 1023 - 1033
4-n-Hexyloxybromobenzene Preparation Products And Raw materials
| Supplier | Tel | Country | ProdList | Advantage | |
|---|---|---|---|---|---|
| J & K SCIENTIFIC LTD. | 18210857532 18210857532 | jkinfo@jkchemical.com | China | 96815 | 76 |
| Alfa Aesar | 400-6106006 | saleschina@alfa-asia.com | China | 30103 | 84 |
| TCI (Shanghai) Development Co., Ltd. | 021-67121386 | Sales-CN@TCIchemicals.com | China | 24512 | 81 |
| Energy Chemical | 400-0056266 | sales8178@energy-chemical.com | China | 44850 | 61 |
| Puyang Huicheng Electronic Material Co. Ltd. | 0393-0393-8910800 15039333257 | info@huichengchem.com | China | 588 | 64 |
| Shandong Xiya Chemical Co., Ltd | 13355009207 13355009207 | 3007715519@qq.com | China | 18722 | 57 |
| Thermo Fisher Scientific | 800-810-5118 | cnchemical@thermofisher.com | China | 17752 | 75 |
| TOKYO CHEMICAL INDUSTRY CO., LTD. | 03-36680489 | Sales-JP@TCIchemicals.com | Japan | 28364 | 80 |
| TCI Europe | 320-37350700 | sales@tcieurope.eu | Europe | 23654 | 75 |
| TCI AMERICA | 800-4238616 | sales@tciamerica.com | Americas | 23636 | 75 |
View Latest Price from 4-n-Hexyloxybromobenzene manufacturers
| Image | Update time | Product | Price | Min. Order | Purity | Supply Ability | Manufacturer | |
|---|---|---|---|---|---|---|---|---|
 |
2019-07-06 | p-Hexyloxybromobenzene
30752-19-3
|
$1.00 | 1KG | 98% | 200kg | Career Henan Chemical Co |
-
- p-Hexyloxybromobenzene
30752-19-3
- $1.00
- 98%
- Career Henan Chemical Co
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