3-Methyl-4-nitrobenzonitrile
- CAS No.
- 96784-54-2
- Chemical Name:
- 3-Methyl-4-nitrobenzonitrile
- Synonyms
- -METHYL-4-NITROBENZO;4-NITRO-M-TOLUNITRILE;5-Cyano-2-nitrotoluene;3-Methyl-4-nitrobenzonitrile;4-Nitro-3-methylbenzonitrile;Benzonitrile, 3-methyl-4-nitro-;3-Methyl-4-nitrobenzonitrile 97%;5-Cyano-2-nitrotoluene, 4-Nitro-m-tolunitrile;5-Cyano-2-nitrotoluene, 4-Cyano-2-methylnitrobenzene
- CBNumber:
- CB6456984
- Molecular Formula:
- C8H6N2O2
- Molecular Weight:
- 162.15
- MDL Number:
- MFCD00017615
- MOL File:
- 96784-54-2.mol
- MSDS File:
- SDS
- TDS File:
- TDS
| Melting point | 81-83°C |
|---|---|
| Boiling point | 322.2±30.0 °C(Predicted) |
| Density | 1.26±0.1 g/cm3(Predicted) |
| storage temp. | Sealed in dry,Room Temperature |
| Appearance | White to light brown Solid |
| Water Solubility | Insoluble in water |
| BRN | 2443778 |
| CAS DataBase Reference | 96784-54-2(CAS DataBase Reference) |
SAFETY
Risk and Safety Statements
| Symbol(GHS) |  GHS06 |
|||||||||
|---|---|---|---|---|---|---|---|---|---|---|
| Signal word | Warning | |||||||||
| Hazard statements | H302-H312-H315-H319-H331-H335 | |||||||||
| Precautionary statements | P261-P280-P304+P340-P305+P351+P338-P405-P501a | |||||||||
| Hazard Codes | T,Xi | |||||||||
| Risk Statements | 20/21/22-36/37/38 | |||||||||
| Safety Statements | 26-36/37/39-45-36 | |||||||||
| RIDADR | 3439 | |||||||||
| Hazard Note | Toxic | |||||||||
| HazardClass | 6.1 | |||||||||
| PackingGroup | III | |||||||||
| HS Code | 2926907090 | |||||||||
| NFPA 704 |
|
3-Methyl-4-nitrobenzonitrile price More Price(44)
| Manufacturer | Product number | Product description | CAS number | Packaging | Price | Updated | Buy |
|---|---|---|---|---|---|---|---|
| Biosynth | FM00512 | 3-Methyl-4-nitrobenzonitrile | 96784-54-2 | 25g | $150 | 2026-06-04 | Buy |
| Biosynth | FM00512 | 3-Methyl-4-nitrobenzonitrile | 96784-54-2 | 5g | $150 | 2026-06-04 | Buy |
| Biosynth | FM00512 | 3-Methyl-4-nitrobenzonitrile | 96784-54-2 | 50g | $162 | 2026-06-04 | Buy |
| Biosynth | FM00512 | 3-Methyl-4-nitrobenzonitrile | 96784-54-2 | 250g | $487.5 | 2026-06-04 | Buy |
| Apolloscientific | OR30256 | 3-Methyl-4-nitrobenzonitrile >98% | 96784-54-2 | 1g | $21 | 2026-06-04 | Buy |
3-Methyl-4-nitrobenzonitrile Chemical Properties, Uses, Production
Uses
3-Methyl-4-nitrobenzonitrile is used to produce 4-amino-3-methyl-benzonitrile.
Synthesis
99584-85-7
96784-54-2
General procedure for the synthesis of 3-methyl-4-nitrobenzonitrile from 3-methyl-4-nitrobenzamide: 3-methyl-4-nitrobenzamide (5 g, 28 mmol) was dissolved in 300 ml of toluene under stirring conditions, followed by the slow addition of phosphorus oxychloride (POCl3, 22 g, 140 mmol). After the addition was completed, the reaction mixture was heated to reflux for 24 hours. Upon completion of the reaction, the mixture was carefully poured into ice water and extracted three times with ethyl acetate. The organic phases were combined, dried with anhydrous sodium sulfate, filtered and concentrated under reduced pressure. Finally, the residue was purified by ethanol recrystallization to afford the target product 3-methyl-4-nitrobenzonitrile (3.2 g, 70% yield).
References
[1] Patent: WO2014/172871, 2014, A1. Location in patent: Page/Page column 88
[2] Justus Liebigs Annalen der Chemie, 1867, vol. 144, p. 182
[3] Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1973, p. 2940 - 2948
[4] Patent: US5034410, 1991, A
3-Methyl-4-nitrobenzonitrile Preparation Products And Raw materials
Raw materials
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Preparation Products
3-Methyl-4-nitrobenzonitrile Suppliers
| Supplier | Tel | Country | ProdList | Advantage | |
|---|---|---|---|---|---|
| J & K SCIENTIFIC LTD. | 18210857532 18210857532 | jkinfo@jkchemical.com | China | 96815 | 76 |
| Meryer (Shanghai) Chemical Technology Co., Ltd. | 4006356688 18621169109 | market03@meryer.com | China | 40202 | 62 |
| Alfa Aesar | 400-6106006 | saleschina@alfa-asia.com | China | 30103 | 84 |
| Energy Chemical | 400-0056266 | sales8178@energy-chemical.com | China | 44850 | 61 |
| Shanghai Hanhong Scientific Co.,Ltd. | 021-54306202 13764082696 | info@hanhongsci.com | China | 42917 | 64 |
| Syntechem Co.,Ltd | info@syntechem.com | China | 12973 | 57 | |
| Sinopharm Chemical Reagent Co,Ltd. | 86-21-63210123 | sj_scrc@sinopharm.com | China | 9791 | 79 |
| Chengdu Ai Keda Chemical Technology Co., Ltd. | 4008-755-333 18080918076 | 800078821@qq.com | China | 9706 | 55 |
| Shanghai Raise Chemical Technology Co.,Ltd | 15026594951 | rs@raise-chem.com | China | 4905 | 55 |
| Nanjing ShengSai Chemical Co., Ltd. | 025-85205967 13951876367 | shengsaichem@163.com | China | 818 | 58 |
View Latest Price from 3-Methyl-4-nitrobenzonitrile manufacturers
| Image | Update time | Product | Price | Min. Order | Purity | Supply Ability | Manufacturer | |
|---|---|---|---|---|---|---|---|---|
 |
2020-01-13 | 3-METHYL-4-NITROBENZONITRILE
96784-54-2
|
$1.00 | 1KG | 99% | 100KG | Career Henan Chemical Co |
-
- 3-METHYL-4-NITROBENZONITRILE
96784-54-2
- $1.00
- 99%
- Career Henan Chemical Co
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