TETRAHYDROTHIOPYRAN-4-OL 97
- CAS No.
- 29683-23-6
- Chemical Name:
- TETRAHYDROTHIOPYRAN-4-OL 97
- Synonyms
- thian-4-ol;4-Hydroxythiane;Thiacyclohexane-4-ol;Tetrahydrothiophene-4-ol;Tetrahydro-2H-thiopyran-4-O;Thiopyran-4-ol, tetrahydro-;4-Hydroxytetrahydrothiopyran;TETRAHYDROTHIOPYRAN-4-OL 97;2H-thiopyran-4-ol, tetrahydro-;4-hydroxy-tetrahydro-2H-thiopyran
- CBNumber:
- CB6499679
- Molecular Formula:
- C5H10OS
- Molecular Weight:
- 118.2
- MDL Number:
- MFCD02942489
- MOL File:
- 29683-23-6.mol
- MSDS File:
- SDS
| Product description | Number | Pack Size | Price |
| Tetrahydrothiopyran-4-ol 97% | 540714 | 1g | $226 |
| Tetrahydro-2H-thiopyran-4-ol >98.0%(GC) | T3373 | 1g | $163 |
| Tetrahydro-2H-thiopyran-4-ol >98.0%(GC) | T3373 | 5g | $810 |
| Tetrahydro-2H-thiopyran-4-ol >99% | OR928607 | 100mg | $21 |
| Tetrahydro-2H-thiopyran-4-ol >99% | OR928607 | 250mg | $24 |
| More product size | |||
| Melting point | 47-51 °C (lit.) |
|---|---|
| Boiling point | 70°C/0.05mmHg(lit.) |
| Density | 1.148±0.06 g/cm3(Predicted) |
| Flash point | >230 °F |
| storage temp. | under inert gas (nitrogen or Argon) at 2-8°C |
| pka | 14.56±0.20(Predicted) |
| form | powder to lump |
| color | White to Almost white |
| InChI | 1S/C5H10OS/c6-5-1-3-7-4-2-5/h5-6H,1-4H2 |
| InChIKey | YODQQARABJQLIP-UHFFFAOYSA-N |
| SMILES | OC1CCSCC1 |
| UNSPSC Code | 12352100 |
| NACRES | NA.22 |
SAFETY
Risk and Safety Statements
| Symbol(GHS) |  GHS07 |
|||||||||
|---|---|---|---|---|---|---|---|---|---|---|
| Signal word | Warning | |||||||||
| Hazard statements | H315-H319-H335 | |||||||||
| Precautionary statements | P261-P305+P351+P338 | |||||||||
| PPE | Eyeshields, Gloves, type N95 (US) | |||||||||
| RIDADR | UN 3335 | |||||||||
| WGK Germany | 3 | |||||||||
| HazardClass | IRRITANT | |||||||||
| HS Code | 2934999090 | |||||||||
| Storage Class | 11 - Combustible Solids | |||||||||
| NFPA 704 |
|
TETRAHYDROTHIOPYRAN-4-OL 97 price More Price(50)
| Manufacturer | Product number | Product description | CAS number | Packaging | Price | Updated | Buy |
|---|---|---|---|---|---|---|---|
| Sigma-Aldrich | 540714 | Tetrahydrothiopyran-4-ol 97% | 29683-23-6 | 1g | $226 | 2023-06-20 | Buy |
| TCI Chemical | T3373 | Tetrahydro-2H-thiopyran-4-ol >98.0%(GC) | 29683-23-6 | 1g | $163 | 2026-04-30 | Buy |
| TCI Chemical | T3373 | Tetrahydro-2H-thiopyran-4-ol >98.0%(GC) | 29683-23-6 | 5g | $810 | 2026-04-30 | Buy |
| Apolloscientific | OR928607 | Tetrahydro-2H-thiopyran-4-ol >99% | 29683-23-6 | 100mg | $21 | 2026-06-04 | Buy |
| Apolloscientific | OR928607 | Tetrahydro-2H-thiopyran-4-ol >99% | 29683-23-6 | 250mg | $24 | 2026-06-04 | Buy |
TETRAHYDROTHIOPYRAN-4-OL 97 Chemical Properties,Uses,Production
Uses
Tetrahydrothiopyran-4-ol is a sulfur containing heterocyclic building block. Tetrahydrothiopyran-4-ol can be synthesized from tetrahydrothiopyran-4-one. It participates in the synthesis of 4-hydroxyl-1-methyltetrahydrothiopyranium iodide.
General Description
Tetrahydrothiopyran-4-ol is a sulfur containing heterocyclic building block. Tetrahydrothiopyran-4-ol can be synthesized from tetrahydrothiopyran-4-one. It participates in the synthesis of 4-hydroxyl-1-methyltetrahydrothiopyranium iodide.
Synthesis
1072-72-6
29683-23-6
GENERAL METHOD: Tetrahydrothiopyran-4-one (40.10 g, 0.271 mol) was dissolved in methanol (700 mL), and sodium borohydride (15.36 g, 0.406 mol) was added in batches under ice-bath cooling, and the reaction was stirred for 1 hr. (NOTE: the reaction is exothermic and violent). Subsequently, the reaction mixture was continued to be stirred at 20°C for 2 hours. After completion of the reaction, the solvent was removed by concentration under reduced pressure to give a solid residue. To the residue was added a mixture of saturated aqueous sodium bicarbonate (150 mL) and ethyl acetate (250 mL) (Note: the product is soluble in water). After vigorous shaking, the organic layer was separated and the aqueous layer was further extracted with ethyl acetate (4 x 250 mL). All organic layers were combined, dried over anhydrous sodium sulfate and concentrated to dryness under reduced pressure to give the target product tetrahydro-2H-thiopyran-4-ol.
References
[1] Synthetic Communications, 2018, vol. 48, # 17, p. 2198 - 2205
[2] Chemistry - A European Journal, 2018, vol. 24, # 62, p. 16526 - 16531
[3] Bulletin of the Chemical Society of Japan, 1995, vol. 68, # 9, p. 2739 - 2750
[4] Chemical Communications (Cambridge, United Kingdom), 2002, # 10, p. 1070 - 1071
[5] Patent: EP3342765, 2018, A1. Location in patent: Paragraph 0337
TETRAHYDROTHIOPYRAN-4-OL 97 Preparation Products And Raw materials
| Supplier | Tel | Country | ProdList | Advantage | |
|---|---|---|---|---|---|
| Shenzhen Nexconn Pharmatechs Ltd | +86-755-89396905 +86-15013857715 | admin@nexconn.com | China | 10403 | 58 |
| Accela ChemBio Inc. | +1-858-6993322 +86-18019713315 | info@accelachem.com | United States | 21193 | 58 |
| CONIER CHEM AND PHARMA LIMITED | sales@conier.com | China | 49979 | 58 | |
| career henan chemical co | +86-0371-86658258 | factory@coreychem.com | China | 29792 | 58 |
| Guangzhou Yuheng Pharmaceutical Technology Co., Ltd | +8613580539051 | joe@yuhengpharm.com | CHINA | 21142 | 58 |
| Hefei TNJ Chemical Industry Co.,Ltd. | +86-0551-65418671 +86-189 4982 3763 | sales@tnjchem.com | China | 34563 | 58 |
| KARMEL TECHNOLOGY (HK) CO.,LIMITED | +8618795957998 | karmelhk@126.com | CHINA | 2886 | 58 |
| Dayang Chem (Hangzhou) Co.,Ltd. | +86-0571-88938639 17705817739 | info@dycnchem.com | China | 52704 | 58 |
| Labnetwork lnc. | +86-27-50766799 +86-18062016861 | contact@labnetwork.com | China | 19987 | 58 |
| Hangzhou MolCore BioPharmatech Co.,Ltd. | +86-057181025280; +8617767106207 | sales@molcore.com | China | 49734 | 58 |
View Lastest Price from TETRAHYDROTHIOPYRAN-4-OL 97 manufacturers
| Image | Update time | Product | Price | Min. Order | Purity | Supply Ability | Manufacturer | |
|---|---|---|---|---|---|---|---|---|
 |
2020-01-03 | TETRAHYDROTHIOPYRAN-4-OL 97
29683-23-6
|
$6.60 | 1KG | 97%-99% | 1kg -1000kg | Career Henan Chemical Co |
-
- TETRAHYDROTHIOPYRAN-4-OL 97
29683-23-6
- $6.60
- 97%-99%
- Career Henan Chemical Co
29683-23-6(TETRAHYDROTHIOPYRAN-4-OL 97)Related Search:
1of4
