1-Ethyl-3-pyrrolidinol
- CAS No.
- 30727-14-1
- Chemical Name:
- 1-Ethyl-3-pyrrolidinol
- Synonyms
- N-Ethyl-3-hydroxypyrrolidine;NSC 88610;Ethylpyrrolidinol;1-ethyl-3-pyrrolidino;1-ethylpyrrolidin-3-ol;1-Ethyl-3-pyrrolidinol;N- Ethyl-3-pyrrolidinol;3-Pyrrolidinol, 1-ethyl-;1-Ethyl-3-pyrrolidinol>1-ETHYL-3-PYRROLIDINOL 95+%
- CBNumber:
- CB9364778
- Molecular Formula:
- C6H13NO
- Molecular Weight:
- 115.17
- MDL Number:
- MFCD00003179
- MOL File:
- 30727-14-1.mol
- MSDS File:
- SDS
- TDS File:
- TDS
| Boiling point | 59-61 °C1 mm Hg(lit.) |
|---|---|
| Density | 0.967 g/mL at 25 °C(lit.) |
| refractive index |
n |
| Flash point | 165 °F |
| storage temp. | Sealed in dry,Room Temperature |
| form | clear liquid |
| pka | 14.83±0.20(Predicted) |
| color | Colorless to Brown |
| InChI | 1S/C6H13NO/c1-2-7-4-3-6(8)5-7/h6,8H,2-5H2,1H3 |
| InChIKey | IDBNECMSCRAUNU-UHFFFAOYSA-N |
| SMILES | CCN1CCC(O)C1 |
| CAS DataBase Reference | 30727-14-1(CAS DataBase Reference) |
| EWG's Food Scores | 1 |
| UNSPSC Code | 12352100 |
SAFETY
Risk and Safety Statements
| Symbol(GHS) |  GHS07 |
|||||||||
|---|---|---|---|---|---|---|---|---|---|---|
| Signal word | Warning | |||||||||
| Hazard statements | H227-H315-H319-H335 | |||||||||
| Precautionary statements | P261-P305+P351+P338-P210-P264-P280-P302+P352+P332+P313+P362+P364-P305+P351+P338+P337+P313-P370+P378-P403+P235-P501 | |||||||||
| target organs | Respiratory system | |||||||||
| PPE | dust mask type N95 (US), Eyeshields, Gloves | |||||||||
| Hazard Codes | Xi | |||||||||
| Risk Statements | 36/37/38 | |||||||||
| Safety Statements | 26-36/37/39 | |||||||||
| WGK Germany | 3 | |||||||||
| RTECS | UY5685500 | |||||||||
| HS Code | 2933998090 | |||||||||
| Storage Class | 11 - Combustible Solids | |||||||||
| Hazard Classifications | Eye Irrit. 2 Skin Irrit. 2 STOT SE 3 |
|||||||||
| Toxicity | mouse,LD50,intravenous,180mg/kg (180mg/kg),U.S. Army Armament Research & Development Command, Chemical Systems Laboratory, NIOSH Exchange Chemicals. Vol. NX#02177, | |||||||||
| NFPA 704 |
|
1-Ethyl-3-pyrrolidinol price More Price(43)
| Manufacturer | Product number | Product description | CAS number | Packaging | Price | Updated | Buy |
|---|---|---|---|---|---|---|---|
| Sigma-Aldrich | E47352 | 1-Ethyl-3-pyrrolidinol 97% | 30727-14-1 | 5g | $422 | 2023-01-07 | Buy |
| TCI Chemical | E0425 | 1-Ethyl-3-pyrrolidinol >95.0%(GC)(T) | 30727-14-1 | 10mL | $73 | 2026-04-30 | Buy |
| Biosynth | FBA72714 | 1-Ethyl-3-pyrrolidinol | 30727-14-1 | 25g | $625 | 2026-06-04 | Buy |
| Apolloscientific | OR920330 | 1-Ethyl-3-pyrrolidinol >98% | 30727-14-1 | 1g | $21 | 2026-06-04 | Buy |
| Apolloscientific | OR920330 | 1-Ethyl-3-pyrrolidinol >98% | 30727-14-1 | 5g | $47 | 2026-06-04 | Buy |
1-Ethyl-3-pyrrolidinol Chemical Properties,Uses,Production
Synthesis
2419-74-1
75-04-7
30727-14-1
The present embodiment is a method for the preparation of 1-ethyl-3-pyrrolidinol, which was carried out as follows: 250 g of 40 wt% aqueous ethylamine solution was added to a 500 mL four-necked flask, cooled to 10 °C, and placed in an ice-water bath. Under stirring conditions, 102 g of 1,4-dichloro-2-butanol was added dropwise, and the temperature was controlled to be about 15 °C. After the dropwise addition was completed in about 15 min, the reaction system was transferred to a 500 mL autoclave, sealed, evacuated to a pressure of 1.0±0.1 MPa, heated to 120±2°C, stirred and reacted for about 10 h. The reaction was monitored by GC until the raw material disappeared. After the reaction was completed, cooled to room temperature, discharged the reaction material, added 110g of sodium hydroxide in batches, taking care to control the temperature below 50°C to release ethylamine gas and precipitate a white solid, and continued stirring for 1h. After filtration, the filtrate was layered, the upper organic phase was taken, 100mL of ethanol and 18g of anhydrous magnesium sulfate were added, and stirred for 2~3h. Filtered again, and the filtrate was concentrated under vacuum to obtain a yellow transparent The filtrate was again filtered and concentrated under vacuum to obtain a yellow transparent oily liquid, and finally 46.7 g of colorless and transparent 1-ethyl-3-pyrrolidinol was obtained by vacuum distillation with a yield of 64.8% and a purity of 99.3% (HPLC).
References
[1] Patent: CN106631956, 2017, A. Location in patent: Paragraph 0022; 0023; 0024; 0025; 0026; 0027
1-Ethyl-3-pyrrolidinol Preparation Products And Raw materials
| Supplier | Tel | Country | ProdList | Advantage | |
|---|---|---|---|---|---|
| J & K SCIENTIFIC LTD. | 18210857532 18210857532 | jkinfo@jkchemical.com | China | 96815 | 76 |
| Meryer (Shanghai) Chemical Technology Co., Ltd. | 4006356688 18621169109 | market03@meryer.com | China | 40202 | 62 |
| TCI (Shanghai) Development Co., Ltd. | 021-67121386 | Sales-CN@TCIchemicals.com | China | 24512 | 81 |
| Energy Chemical | 400-0056266 | sales8178@energy-chemical.com | China | 44850 | 61 |
| Adamas Reagent, Ltd. | 400-6009262 15618770481 | yhx@titansci.com | China | 14098 | 59 |
| Shanghai Longsheng chemical Co.,Ltd. | 58099637 13585536065 | sales@shlschem.com | China | 9880 | 59 |
| China DongFan Chemical Co.,LTD | 86-0571-85151182 | China | 5681 | 66 | |
| Shandong Xiya Chemical Co., Ltd | 13355009207 13355009207 | 3007715519@qq.com | China | 18722 | 57 |
| Maya High Purity Chemicals | +86 (573) 82222445 (0)18006601000 452520369 | sales@maya-r.com | China | 11693 | 57 |
| TOKYO CHEMICAL INDUSTRY CO., LTD. | 03-36680489 | Sales-JP@TCIchemicals.com | Japan | 28364 | 80 |
View Lastest Price from 1-Ethyl-3-pyrrolidinol manufacturers
| Image | Update time | Product | Price | Min. Order | Purity | Supply Ability | Manufacturer | |
|---|---|---|---|---|---|---|---|---|
 |
2019-09-02 | 1-ETHYL-3-PYRROLIDINOL
30727-14-1
|
$1.00 | 1KG | ≥98% | 200kg | Career Henan Chemical Co |
-
- 1-ETHYL-3-PYRROLIDINOL
30727-14-1
- $1.00
- ≥98%
- Career Henan Chemical Co
