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4-Benzyloxybenzaldehyde

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Products Intro: Product Name:4-Benzyloxybenzaldehyde
CAS:4397-53-9
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Products Intro: Product Name:4-Benzyloxybenzaldehyde
CAS:4397-53-9
Purity:98%(Min,HPLC) Package:100g;1kg;5kg,10kg,25kg,50kg
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Products Intro: Product Name:4-Benzyloxybenzaldehyde
CAS:4397-53-9
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CAS:4397-53-9
Purity:99% Package:25KG;5KG;1KG
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Products Intro: Product Name:4-Benzyloxybenzaldehyde
CAS:4397-53-9
Purity:98% Package:10kg;1kg;100g;10g

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4-Benzyloxybenzaldehyde Basic information
Product Name:4-Benzyloxybenzaldehyde
Synonyms:AKOS AU36-M28;AKOS BBS-00003143;4-(Phenylmethoxy)benzaldehyde;Benzaldehyde, 4-(phenylmethoxy)-;Benzaldehyde, p-(benzyloxy)-;LABOTEST-BB LT00233210;ASISCHEM R39515;TIMTEC-BB SBB000526
CAS:4397-53-9
MF:C14H12O2
MW:212.24
EINECS:224-527-2
Product Categories:Aromatics;Intermediates & Fine Chemicals;Pharmaceuticals;FINE Chemical & INTERMEDIATES;Aromatic Aldehydes & Derivatives (substituted);Benzaldehyde (Building Blocks for Liquid Crystals);Building Blocks for Liquid Crystals;Functional Materials;Aldehydes;C10 to C21;Carbonyl Compounds
Mol File:4397-53-9.mol
4-Benzyloxybenzaldehyde Structure
4-Benzyloxybenzaldehyde Chemical Properties
Melting point 71-74 °C (lit.)
Boiling point 197-199 °C (11 mmHg)
density 1.1035 (rough estimate)
refractive index 1.6000 (estimate)
Fp 197-199°C/20mm
storage temp. Keep in dark place,Sealed in dry,Room Temperature
solubility Chloroform (Slightly), Ethyl Acetate (Sparingly)
form Crystalline Powder
color Creamish to yellow
Water Solubility insoluble
Sensitive Air Sensitive
BRN 1242385
InChI1S/C14H12O2/c15-10-12-6-8-14(9-7-12)16-11-13-4-2-1-3-5-13/h1-10H,11H2
InChIKeyZVTWZSXLLMNMQC-UHFFFAOYSA-N
SMILES[H]C(=O)c1ccc(OCc2ccccc2)cc1
LogP3.360 (est)
CAS DataBase Reference4397-53-9(CAS DataBase Reference)
NIST Chemistry ReferenceBenzyl 4-formylphenyl ether(4397-53-9)
EPA Substance Registry SystemBenzaldehyde, 4-(phenylmethoxy)- (4397-53-9)
Safety Information
Safety Statements 24/25
WGK Germany 3
9-23
TSCA TSCA listed
HazardClass IRRITANT
HS Code 29124900
Storage Class11 - Combustible Solids
MSDS Information
ProviderLanguage
4-Benzyloxybenzaldehyde English
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4-Benzyloxybenzaldehyde Usage And Synthesis
Chemical Propertiescreamish to yellow crystalline powder
Uses4-Benzyloxybenzaldehyde is a position isomer of the adenylyl cyclase activator 2-Benzyloxybenzaldehyde. 4-Benzyloxybenzaldehyde also has much less potent anticancer activity against HL-60 cells that i ts isomeric counterpart.
Uses4-Benzyloxybenzaldehyde is used in the synthesis of (5-fluoro-(2R*,3S*)-2,3-bis(4-hydroxyphenyl)pentanenitrile),an estrogen receptor β-selective ligand. It is a position isomer of the adenylyl cyclase activator 2-benzyloxybenzaldehyde.
Synthesis Reference(s)Journal of Medicinal Chemistry, 32, p. 192, 1989 DOI: 10.1021/jm00121a035
General Description4-(Benzyloxy)benzaldehyde was used in the synthesis of (5-fluoro-(2R*,3S*)-2,3-bis(4-hydroxyphenyl)pentanenitrile),an estrogen receptor β-selective ligand.
SynthesisP-hydroxybenzaldehyde 5g (41mmol) and potassium carbonate 11.3g into a three-necked flask, add N, N-dimethylformamide (DMF) 25ml, stirring for 15min to form a suspension, dropwise addition of benzyl chloride 5.7g (45mmol), the reaction at room temperature of 6-8h, TLC tracking reaction to the end of the ice-water mixture was poured into a large number of solids precipitation, filtration, washed a number of times with water. Filtered, washed with water for several times, dried to obtain a white solid 4-benzyloxybenzaldehyde 8.13g (yield 94%).
Tag:4-Benzyloxybenzaldehyde(4397-53-9) Related Product Information
4-Methoxybenzylchloride 4-Hydroxybenzaldehyde 4-Dimethylaminobenzaldehyde p-Anisaldehyde 3-(Trifluoromethyl)benzaldehyde Monobenzone 2-Nitrobenzaldehyde Benzaldehyde o-Anisaldehyde 3-(METHOXYMETHOXY)BENZALDEHYDE 5-(4-FLUOROPHENYL)VALERIC ACID ent-EzetiMibe EzetiMibe (3R,4R,3'S)-IsoMer (R)-3-((S)-5-(4-fluorophenyl)-5-hydroxypentanoyl)-4-phenyloxazolidin-2-one (3R,4R)-1-(4-fluorophenyl)-3-((R)-3-(4-fluorophenyl)-3-hydroxypropyl)-4-(4-hydroxyphenyl)azetidin-2-one (4S)-3-(2,2-dimethylpropanoyl)-4-phenyl-1,3-oxazolidin-2-one 4-BENZOYLBUTYRIC ACID 5-(2-FLUOROPHENYL)-5-OXOVALERIC ACID