2-Chloro-6-methylphenol

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2-Chloro-6-methylphenol Basic information
Product Name:2-Chloro-6-methylphenol
Synonyms:6-CHLORO-O-CRESOL;2-Methyl-6-chlorophenol;6-chloro-o-creso;o-Cresol, 6-chloro-;2-Chloro-6-methylphenol,98%;2-Chloro-6-methylphenol, tech;6-CHLORO-ORTHO-CRESOL;6-CHLORO-2-METHYLPHENOL
CAS:87-64-9
MF:C7H7ClO
MW:142.58
EINECS:201-760-8
Product Categories:Phenol&Thiophenol&Mercaptan;Chlorine Compounds;Phenols
Mol File:87-64-9.mol
2-Chloro-6-methylphenol Structure
2-Chloro-6-methylphenol Chemical Properties
Melting point 130 °C
Boiling point 86 °C
density 1,201 g/cm3
refractive index 1.5450
Fp 72°C
storage temp. Sealed in dry,Room Temperature
pka8.84±0.10(Predicted)
AppearanceColorless to light yellow Liquid
Water Solubility Soluble in water (24 mg/ml at 25°C).
BRN 774623
CAS DataBase Reference87-64-9(CAS DataBase Reference)
EPA Substance Registry System6-Chloro-o-cresol (87-64-9)
Safety Information
Hazard Codes Xi,Xn
Risk Statements 21/22-36/38-36/37/38-22-38
Safety Statements 26-28-36/37/39-23
RIDADR 3437
RTECS GO7120100
Hazard Note Irritant
HazardClass 6.1
PackingGroup II
HS Code 2908190090
MSDS Information
ProviderLanguage
ALFA English
2-Chloro-6-methylphenol Usage And Synthesis
Chemical PropertiesColoroless to yellow liquid
Uses2-Chloro-6-methylphenol is s an important raw material and intermediate used in Organic Synthesis, Pharmaceuticals, Agrochemicals and Dyestuffs.
Synthesis
o-Cresol

95-48-7

4-Chloro-2-methylphenol

1570-64-5

2-CHLORO-6-METHYLPHENOL

87-64-9

GENERAL METHOD: Molten o-cresol or m-cresol (5.41 g, 50.0 mmol), AlCl3 (0.25 g), and catalyst (100 mg) were added to a dry 50 mL round bottom flask. Thionyl chloride (4.66 mL, 57.7 mmol) was added slowly and dropwise over a period of 2 h via a pressure-equilibrated dropping funnel. The reaction mixture was stirred continuously for 2 hours and then the reaction was quenched with 20 mL of water. The reaction mixture was post-treated by drying the crude product to constant weight and subsequently analyzed by quantitative gas chromatography (GC).

References[1] Synthetic Communications, 2002, vol. 32, # 2, p. 279 - 286
[2] Synlett, 2011, # 11, p. 1537 - 1542
[3] Journal of the Chemical Society, Chemical Communications, 1980, # 1, p. 8 - 9
[4] Zhurnal Russkago Fiziko-Khimicheskago Obshchestva, 1928, vol. 60, p. 161
2-Chloro-6-methylphenol Preparation Products And Raw materials
Raw materialso-Cresol-->Aluminum chloride-->Sulfuryl chloride-->1,2-Dithiolane
Preparation Products(R)-2-Amino-6-methylheptane, 98% e.e., 95-->(R)-(-)-2-Aminoheptane-->4-Bromo-2-chloro-6-methylphenol
Tag:2-Chloro-6-methylphenol(87-64-9) Related Product Information
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