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(S)-(+)-2-(Anilinomethyl)pyrrolidine

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(S)-(+)-2-(Anilinomethyl)pyrrolidine Basic information
Product Name:(S)-(+)-2-(Anilinomethyl)pyrrolidine
Synonyms:2-PyrrolidineMethanaMine,N-phenyl-, (2S)-;(S)-N-(Pyrrolidin-2-ylMethyl)aniline;(2S)-(Anilinomethyl)pyrrolidine;(S)-2-(Phenylaminomethyl)pyrrolidine;(S)-(+)-2-(Anilinomethyl)pyrrolidine 96%;(S)-2-(Anilinomethyl)pyrrolidine,99%e.e.;(S)-(+)-N-(2-PYRROLIDINOMETHYL)ANILINE;(2S)-PHENYL-PYRROLIDIN-2-YLMETHYL-AMINE
CAS:64030-44-0
MF:C11H16N2
MW:176.26
EINECS:
Product Categories:chiral;Asymmetric Synthesis;Synthetic Organic Chemistry;Asymmetric Synthesis;Chiral Catalysts, Ligands, and Reagents;Proline-Based Organocatalysts
Mol File:64030-44-0.mol
(S)-(+)-2-(Anilinomethyl)pyrrolidine Structure
(S)-(+)-2-(Anilinomethyl)pyrrolidine Chemical Properties
Melting point 19°C
Boiling point 111-112 °C/0.55 mmHg (lit.)
density 1.046 g/mL at 25 °C (lit.)
refractive index 1.5750
Fp >230 °F
storage temp. Keep in dark place,Inert atmosphere,Room temperature
solubility sol ether, THF.
form clear liquid
pka10.52±0.10(Predicted)
color Colorless to Yellow to Green
Optical Rotation[α]20/D +19°, c = 1 in ethanol
Sensitive Air Sensitive
BRN 472065
CAS DataBase Reference64030-44-0(CAS DataBase Reference)
Safety Information
Hazard Codes C
Risk Statements 34
Safety Statements 26-36/37/39-45
RIDADR UN 3267 8/PG 2
WGK Germany 3
HazardClass 8
PackingGroup III
HS Code 29339900
MSDS Information
ProviderLanguage
SigmaAldrich English
ALFA English
(S)-(+)-2-(Anilinomethyl)pyrrolidine Usage And Synthesis
Chemical PropertiesClear colorless viscous liquid
Synthesis (S)-2-(Anilinomethyl)pyrrolidine is prepared by the reaction of (S)-N-(benzyloxycarbonyl)proline with ethyl  chloroformate and N-methylmorpholine, aniline, hydrogenolysis with Pd/C, and reduction with LiAlH4 affords the title compound in 59% overall yield.
(S)-(+)-2-(Anilinomethyl)pyrrolidine Preparation Products And Raw materials
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(S)-(+)-2-(Anilinomethyl)pyrrolidine GLY-PRO P-NITROANILIDE P-TOLUENESULFONATE SALT PYR-PNA (S)-(+)-2-(2,6-XYLIDINOMETHYL)PYRROLIDINE (R)-(-)-2-(ANILINOMETHYL)PYRROLIDINE H-PRO-4M-BETANA HCL L-PYROGLUTAMIC ACID BETA-NAPHTHYLAMIDE Z-Gly-Pro-βNA H-PRO-PNA HBR GLY-PRO-MCA TOSYLATE PYR-HIS-PRO-BETANA GLY-PRO 4-METHOXY-BETA-NAPHTHYLAMIDE HYDROCHLORIDE Z-Gly-Pro-PNA Gly-Pro 4-methoxy-beta-naphthylamide Suc-Gly-Pro-AMC Z-Gly-Pro-AMC L-Proline beta-naphthylamide hydrochloride Z-Pro-betana