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| | 2-Amino-N-methyl-acetamide Basic information |
| Product Name: | 2-Amino-N-methyl-acetamide | | Synonyms: | N~1~-methylglycinamide hydrochloride;Aminoacetic acid methyl amide;Einecs 244-934-9;N~1~-methylglycinamide(SALTDATA: HCl);Glycine MethylaMide;Acetamide, 2-amino-N-methyl- | | CAS: | 22356-89-4 | | MF: | C3H8N2O | | MW: | 88.11 | | EINECS: | 244-934-9 | | Product Categories: | | | Mol File: | 22356-89-4.mol |  |
| | 2-Amino-N-methyl-acetamide Chemical Properties |
| Boiling point | 275.6±23.0 °C(Predicted) | | density | 1.005±0.06 g/cm3(Predicted) | | storage temp. | Keep in dark place,Sealed in dry,Room Temperature | | pka | 15.37±0.46(Predicted) |
| | 2-Amino-N-methyl-acetamide Usage And Synthesis |
| Synthesis | The general procedure for the synthesis of 2-amino-N-methylacetamide from compound 12a (CAS:21855-72-1) was as follows: 10% Pd/C catalyst was added to a methanol (10 mL) solution of compound 12a (170 mg, 0.77 mmol). The hydrogenation reaction was carried out at room temperature and atmospheric pressure for 3 hours. Upon completion of the reaction, the catalyst was removed by diatomaceous earth filtration and the resulting clarified solution was dried to give 2-amino-N-methylacetamide as an oily product. The yield was 97%. The molecular formula is C3H9N2O. | | References | [1] Patent: WO2006/103463, 2006, A1. Location in patent: Page/Page column 15; Figure 3
[2] Bioorganic and Medicinal Chemistry, 2011, vol. 19, # 3, p. 1285 - 1297
[3] Journal of Organic Chemistry, 1977, vol. 42, # 12, p. 2105 - 2108
[4] Synthesis, 1977, p. 478 - 480 |
| | 2-Amino-N-methyl-acetamide Preparation Products And Raw materials |
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