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ChemicalBook CAS DataBase List 2-(Chloroacetyl)-6,7-dimethoxy-1,2,3,4-tetrahydroisoquinoline
111631-72-2

2-(Chloroacetyl)-6,7-dimethoxy-1,2,3,4-tetrahydroisoquinoline synthesis

6synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1.1: ethanol / 2 h / 20 °C
1.2: 6 h / Reflux
2.1: potassium carbonate / dichloromethane / 2 h / 20 °C / Cooling with ice

References:

Xing, Junhao;Li, Qing;Zhang, Shengping;Liu, Haomiao;Zhao, Leilei;Cheng, Haibo;Zhang, Yuan;Zhou, Jinpei;Zhang, Huibin [Chemical Biology and Drug Design,2014,vol. 84,# 3,p. 364 - 377]