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ChemicalBook CAS DataBase List 2,2-Diethoxyethylamine
645-36-3

2,2-Diethoxyethylamine synthesis

14synthesis methods

There are two main methods of synthesizing aminoacetaldehyde diethyl acetal as follows:

(1) 2-(2-azidoethyl)-1,3-dioxolane is generated from 2-(2-azidoethyl)-1,3-dioxolane by refluxing 2-(2-azidoethyl)-1,3-dioxolane with sodium azide over a pha

-

Yield:-

Steps:

Multi-step reaction with 2 steps
1: durch Bromierung
2: alcohol; ammonia / 110 - 115 °C

References:

Hartung;Adkins [Journal of the American Chemical Society,1927,vol. 49,p. 2518]

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