Methyl 4-methylbenzoate synthesis
- Product Name:Methyl 4-methylbenzoate
- CAS Number:99-75-2
- Molecular formula:C9H10O2
- Molecular Weight:150.17
67-56-1
788 suppliers
$7.30/5ml-f
104-87-0
514 suppliers
$6.00/25g
99-75-2
283 suppliers
$6.00/10g
106-44-5
504 suppliers
$14.00/5g
Yield:99-75-2 75% ，106-44-5 15%
Reaction Conditions:
with diphenyl diselenide;dihydrogen peroxide at 50; for 2 h;Green chemistry;
Steps:
3.3. General Procedure for the Synthesis of Esters 6
General procedure: Diphenyl diselenide (3, 0.006 g; 0.02 mmol) was treated with H2O2 (30%·w/w, 0.15 mL, 1.5 mmol)and stirred at room temperature until the discoloration of the reaction mixture. Then, the aldehyde 1(1 mmol) and the appropriate alcohol (2.5 mmol) were added. The reaction mixture was stirred at50 °C for 2 h and extracted three times with EtOAc (3 × 20 mL). The collected organic layers were driedover Na2SO4 and the solvent evaporated under reduced pressure.
References:
Sancineto, Luca;Tidei, Caterina;Bagnoli, Luana;Marini, Francesca;Lenardo, Eder J.;Santi, Claudio [Molecules,2015,vol. 20,# 6,p. 10496 - 10510]
67-56-1
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$7.30/5ml-f
201230-82-2
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106-38-7
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$14.00/5g
99-75-2
283 suppliers
$6.00/10g
6908-41-4
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$17.00/25g
99-75-2
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$6.00/10g
2527-96-0
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$12.00/250mg
74-85-1
113 suppliers
$79.00/11l
99-75-2
283 suppliers
$6.00/10g
