N,N-Diisopropyl-P,P-diphenylphosphinicamide synthesis
- Product Name:N,N-Diisopropyl-P,P-diphenylphosphinicamide
- CAS Number:131173-04-1
- Molecular formula:C18H24NOP
- Molecular Weight:301.36
Yield:-
Steps:
Multi-step reaction with 2 steps
1: copper(I) tetrakis(acetonitrile)tetrafluoroborate; Cs2CO3 / tetrahydrofuran / 12 h / 20 °C / Schlenk technique; Glovebox; Inert atmosphere
2: dihydrogen peroxide / tetrahydrofuran; water monomer / 0.5 h / 20 °C / Schlenk technique; Glovebox; Inert atmosphere
References:
Li, Yan-Bo;Tian, Hu;Xiao, Jun-Zhao;Yin, Liang;Zhang, Shuai [Angewandte Chemie - International Edition,2022,vol. 61,# 13,art. no. E202117760][Angew. Chem.,2022,vol. 134,# 13]
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