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4-Iodo-2-nitroanisole

4-Iodo-2-nitroanisole Structure
4-Iodo-2-nitroanisole structure
CAS No.
52692-09-8
Chemical Name:
4-Iodo-2-nitroanisole
Synonyms
4-IODO-2-NITROANISOLE;4-iodo-1-methoxy-2-nitrobenzene;Benzene, 4-iodo-1-methoxy-2-nitro-
CBNumber:
CB3213674
Molecular Formula:
C7H6INO3
Molecular Weight:
279.03
MDL Number:
MFCD08060933
MOL File:
52692-09-8.mol
MSDS File:
SDS
Last updated:2026-05-28 01:03:44
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4-Iodo-2-nitroanisole Properties

Melting point 96-98°C
Boiling point 330.8±27.0 °C(Predicted)
Density 1.893±0.06 g/cm3(Predicted)
storage temp. 2-8°C, protect from light
Appearance Light yellow to yellow Solid
Sensitive Light Sensitive

SAFETY

Risk and Safety Statements

Symbol(GHS)  Skull and Crossbones (GHS06)
GHS06
Signal word  Warning
Hazard statements  H301-H315-H319-H335
Precautionary statements  P261-P280a-P301+P310a-P305+P351+P338-P405-P501a
Risk Statements  23/24/25
Safety Statements  36/37-45
HS Code  2909309090
NFPA 704
1
2 0

4-Iodo-2-nitroanisole price More Price(32)

Manufacturer Product number Product description CAS number Packaging Price Updated Buy
Apolloscientific OR400184 4-Iodo-2-nitroanisole 97% 52692-09-8 250mg $21 2026-06-04 Buy
Apolloscientific OR400184 4-Iodo-2-nitroanisole 97% 52692-09-8 1g $24 2026-06-04 Buy
Apolloscientific OR400184 4-Iodo-2-nitroanisole 97% 52692-09-8 5g $48 2026-06-04 Buy
Apolloscientific OR400184 4-Iodo-2-nitroanisole 97% 52692-09-8 25g $192 2026-06-04 Buy
Activate Scientific AS42151 4-Iodo-1-methoxy-2-nitrobenzene 98% 52692-09-8 1g $42 2026-06-04 Buy
Product number Packaging Price Buy
OR400184 250mg $21 Buy
OR400184 1g $24 Buy
OR400184 5g $48 Buy
OR400184 25g $192 Buy
AS42151 1g $42 Buy

4-Iodo-2-nitroanisole Chemical Properties,Uses,Production

Synthesis Reference(s)

Tetrahedron Letters, 10, p. 2427, 1969 DOI: 10.1017/S0009838800024678

Synthesis

2-Nitroanisole

91-23-6

4-Iodo-2-nitroanisole

52692-09-8

General procedure for the synthesis of 4-iodo-2-nitroanisole from 2-nitroanisole: To a stirred solution of 2-nitroanisole (1 mmol) in dichloromethane (CH2Cl2) or 1,2-dichloroethane ((CH2Cl)2) (0.1 M) was added sequentially Ph3PAuNTf2 (0.025 mmol, 19 mg; if using the 2:1 complex of Ph3PAuNTf2 with toluene) and N-iodosuccinimide (NIS, 1.1 mmol, 248 mg). The reaction mixture was stirred at room temperature or reacted under reflux conditions until complete conversion of the feedstock was confirmed by thin layer chromatography (TLC) monitoring. Upon completion of the reaction, the solvent was evaporated under reduced pressure and the resulting crude product was purified by fast column chromatography using different ratios of hexane and ethyl acetate (EtOAc) as eluents, resulting in pure 4-iodo-2-nitroanisole.

References

[1] Synlett, 2014, vol. 25, # 3, p. 399 - 402
[2] Journal of Organic Chemistry, 1990, vol. 55, # 11, p. 3552 - 3555
[3] Tetrahedron, 2004, vol. 60, # 41, p. 9113 - 9119
[4] Synthetic Communications, 2007, vol. 37, # 8, p. 1259 - 1265
[5] Synthesis, 2006, # 7, p. 1195 - 1199

4-Iodo-2-nitroanisole Preparation Products And Raw materials

Raw materials

2-Nitroanisole 4-Iodoanisole 3-Methoxy-2-nitrobenzoic acid 1,2-Dichloroethane N-Iodosuccinimide
Toluene Triphenylphosphine GOLD

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Preparation Products

4-Iodo-2-nitroanisole Suppliers

Global( 91)Suppliers
Supplier Tel Email Country ProdList Advantage
Alfa Aesar 400-6106006 saleschina@alfa-asia.com China 30103 84
Energy Chemical 400-0056266 sales8178@energy-chemical.com China 44850 61
Adamas Reagent, Ltd. 400-6009262 15618770481 yhx@titansci.com China 14098 59
Shanghai Longsheng chemical Co.,Ltd. 58099637 13585536065 sales@shlschem.com China 9880 59
Shandong Xiya Chemical Co., Ltd 13355009207 13355009207 3007715519@qq.com China 18722 57
Shanghai Topbiochem Technology Co., Ltd 021-58170097 info@topbiochem.com China 9513 58
Candia Thamtech Company Limited 0371-86615086 18203638366 0371-86159066 13526786601 China 2011 60
Shanghai Aladdin Bio-Chem Technology Co.,LTD 400-6206333 13167063860 anhua.mao@aladdin-e.com China 29985 65
Bide Pharmatech Ltd. 400-164-7117 18317119277 product02@bidepharm.com China 40000 60
Shanghai HuanChuan Industry Co.,Ltd. 021-61478794 sales@hcshhai.com China 9781 50
Supplier Advantage
Alfa Aesar 84
Energy Chemical 61
Adamas Reagent, Ltd. 59
Shanghai Longsheng chemical Co.,Ltd. 59
Shandong Xiya Chemical Co., Ltd 57
Shanghai Topbiochem Technology Co., Ltd 58
Candia Thamtech Company Limited 60
Shanghai Aladdin Bio-Chem Technology Co.,LTD 65
Bide Pharmatech Ltd. 60
Shanghai HuanChuan Industry Co.,Ltd. 50

View Lastest Price from 4-Iodo-2-nitroanisole manufacturers

Image Update time Product Price Min. Order Purity Supply Ability Manufacturer
4-Iodo-2-nitroanisole pictures 2019-12-25 4-Iodo-2-nitroanisole
52692-09-8
 $1.00 1KG 99% Career Henan Chemical Co

4-Iodo-2-nitroanisole Spectrum

4-Iodo-2-nitroanisole(52692-09-8)1HNMR

52692-09-8(4-Iodo-2-nitroanisole)Related Search:

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4-IODO-2-NITROANISOLE 4-iodo-1-methoxy-2-nitrobenzene Benzene, 4-iodo-1-methoxy-2-nitro- 52692-09-8