2,4-Dichloro-alpha-methylbenzyl alcohol
- CAS No.
- 1475-13-4
- Chemical Name:
- 2,4-Dichloro-alpha-methylbenzyl alcohol
- Synonyms
- 2,4-Dichloro-α1-(2,4-Dichlorophenyl)ethanol;1-(2,4-Dichlorophenyl)ethyl Alcohol;2,4-DICHLORO-A-METHYLBENZYL ALCOHOL;2,4-Dichloro-α-methylbenzyl Alcohol;2,4-Dichloro-±-methylbenzyl Alcohol;2,4-Dichloro-α-methylbenzyl Alcohol;2,4-Dichloro-α-methylbenzenemethanol;2,4-DICHLORO-ALPHA-METHYBENZYLALCOHOL;Benzenemethanol, 2,4-dichloro-α-methyl-
- CBNumber:
- CB4292845
- Molecular Formula:
- C8H8Cl2O
- Molecular Weight:
- 191.05
- MDL Number:
- MFCD00004511
- MOL File:
- 1475-13-4.mol
- MSDS File:
- SDS
| Boiling point | 125-126 °C (7 mmHg) |
|---|---|
| Density | 1.29 |
| refractive index | 1.559-1.561 |
| Flash point | 108 °C |
| storage temp. | Inert atmosphere,Room Temperature |
| pka | 13.67±0.20(Predicted) |
| form | Liquid |
| Specific Gravity | 1.293 |
| color | Clear colorless |
| FDA UNII | D44O14048Q |
SAFETY
Risk and Safety Statements
| Symbol(GHS) | ![]() GHS07 |
|---|---|
| Signal word | Warning |
| Hazard statements | H315-H319-H335 |
| Precautionary statements | P280-P302+P352-P305+P351+P338-P261 |
| Hazard Codes | Xi |
| Risk Statements | 36/37/38 |
| Safety Statements | 37/39-26 |
| HS Code | 29062900 |
2,4-Dichloro-alpha-methylbenzyl alcohol price More Price(35)
| Manufacturer | Product number | Product description | CAS number | Packaging | Price | Updated | Buy |
|---|---|---|---|---|---|---|---|
| Sigma-Aldrich | S463965 | 2,4-DICHLORI-ALPHA-METHYLBENZYL ALCOHOL AldrichCPR | 1475-13-4 | 1 unit | $32.7 | 2026-04-30 | Buy |
| TCI Chemical | D4508 | 2,4-Dichloro-alpha-methylbenzyl Alcohol >98.0%(GC) | 1475-13-4 | 5g | $21 | 2026-04-30 | Buy |
| TCI Chemical | D4508 | 2,4-Dichloro-alpha-methylbenzyl Alcohol >98.0%(GC) | 1475-13-4 | 25g | $65 | 2026-04-30 | Buy |
| Biosynth | BAA47513 | 2,4-Dichloro-±-methylbenzyl Alcohol | 1475-13-4 | 0.25g | $250 | 2026-06-04 | Buy |
| Biosynth | BAA47513 | 2,4-Dichloro-±-methylbenzyl Alcohol | 1475-13-4 | 2.5g | $906.25 | 2026-06-04 | Buy |
2,4-Dichloro-alpha-methylbenzyl alcohol Chemical Properties,Uses,Production
Chemical Properties
clear colorless liquid
Synthesis
2234-16-4
1475-13-4
Sodium borohydride (0.33 g) was slowly added to a methanolic solution (15 ml) of 2,4-dichloroacetophenone (3.0 g) under cooling conditions in an ice bath. The reaction mixture was stirred at room temperature for 30 min before the reaction was terminated by the addition of water (30 ml) followed by extraction with ethyl acetate (30 ml x 2). The organic layers were combined, washed with saturated brine, dried over anhydrous magnesium sulfate, filtered and concentrated under reduced pressure. The crude product was purified by silica gel column chromatography using ethyl acetate-hexane (2:1, v/v) as eluent to afford 1-(2,4-dichlorophenyl)ethanol as a colorless oil (3.00 g, 99% yield).1H-NMR (300 MHz, CDCl3) δ: 1.47 (3H, d, J=6.2 Hz), 1.94 (1H, d, J=3.6 Hz ), 5.25 (1H, qd, J=6.3,3.9Hz), 7.23-7.37 (2H, m), 7.55 (1H, d, J=8.0Hz).
References
[1] Patent: EP1829863, 2007, A1
[2] Patent: WO2006/57448, 2006, A1. Location in patent: Page/Page column 116-117
[3] Zhurnal Obshchei Khimii, 1952, vol. 22, p. 489; engl. Ausg. S. 551
[4] Journal of the Chemical Society, Dalton Transactions, 2001, # 20, p. 2989 - 2995
[5] Advanced Synthesis and Catalysis, 2010, vol. 352, # 10, p. 1779 - 1783
2,4-Dichloro-alpha-methylbenzyl alcohol Preparation Products And Raw materials
Raw materials
Preparation Products
| Supplier | Tel | Country | ProdList | Advantage | |
|---|---|---|---|---|---|
| J & K SCIENTIFIC LTD. | 18210857532 18210857532 | jkinfo@jkchemical.com | China | 96815 | 76 |
| Meryer (Shanghai) Chemical Technology Co., Ltd. | 4006356688 18621169109 | market03@meryer.com | China | 40202 | 62 |
| TCI (Shanghai) Development Co., Ltd. | 021-67121386 | Sales-CN@TCIchemicals.com | China | 24512 | 81 |
| Beijing Ouhe Technology Co., Ltd | 13552068683 13522913783 | 2355560935@qq.com | China | 11777 | 60 |
| Adamas Reagent, Ltd. | 400-6009262 15618770481 | yhx@titansci.com | China | 14098 | 59 |
| RYSS TECH LTD | 400-188-0725 +86 21 34310725 13611771617 | China | 1999 | 57 | |
| Shanghai civi chemical technology co.,Ltd | 86-21-34053660 | sale@labgogo.com | China | 9853 | 52 |
| Thermo Fisher Scientific | 800-810-5118 | cnchemical@thermofisher.com | China | 17752 | 75 |
| TOKYO CHEMICAL INDUSTRY CO., LTD. | 03-36680489 | Sales-JP@TCIchemicals.com | Japan | 28364 | 80 |
| TCI Europe | 320-37350700 | sales@tcieurope.eu | Europe | 23654 | 75 |
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