2,3-DIBROMO-5-NITRO PYRIDINE
- CAS No.
- 15862-36-9
- Chemical Name:
- 2,3-DIBROMO-5-NITRO PYRIDINE
- Synonyms
- 2,3-DIBROMO-5-NITRO PYRIDINE;Pyridine, 2,3-dibromo-5-nitro-;2,3-DIBROMO-5-NITRO PYRIDINE ISO 9001:2015 REACH
- CBNumber:
- CB9268393
- Molecular Formula:
- C5H2Br2N2O2
- Molecular Weight:
- 281.89
- MDL Number:
- MFCD00233994
- MOL File:
- 15862-36-9.mol
SAFETY
Risk and Safety Statements
Symbol(GHS) | ![]() GHS07 |
---|---|
Signal word | Warning |
Hazard statements | H302-H315-H319-H335 |
Precautionary statements | P261-P305+P351+P338 |
Hazard Codes | Xn |
Risk Statements | 20/21/22-36/37/38 |
Safety Statements | 26-36 |
HS Code | 2933399990 |
2,3-DIBROMO-5-NITRO PYRIDINE price More Price(27)
Manufacturer | Product number | Product description | CAS number | Packaging | Price | Updated | Buy |
---|---|---|---|---|---|---|---|
TRC | D426035 | 2,3-Dibromo-5-nitropyridine | 15862-36-9 | 250mg | $55 | 2021-12-16 | Buy |
TRC | D426035 | 2,3-Dibromo-5-nitropyridine | 15862-36-9 | 500mg | $65 | 2021-12-16 | Buy |
AK Scientific | W3443 | 2,3-Dibromo-5-nitropyridine | 15862-36-9 | 1g | $72 | 2021-12-16 | Buy |
Biosynth Carbosynth | FD139764 | 2,3-Dibromo-5-nitropyridine | 15862-36-9 | 5G | $93 | 2021-12-16 | Buy |
Matrix Scientific | 076448 | 2,3-Dibromo-5-nitropyridine 95+% | 15862-36-9 | 1g | $139 | 2021-12-16 | Buy |
2,3-DIBROMO-5-NITRO PYRIDINE Chemical Properties,Uses,Production
Uses
2,3-Dibromo-5-nitropyridine
Synthesis

15862-33-6

15862-36-9
Using 3-bromo-5-nitropyridin-2-ol (9.13 mmol, 2 g) as starting material, 2,3-dibromo-5-nitropyridine (2.23 g, 87% yield) was obtained by the reaction according to the synthesis of Intermediate 2 (Step B). The product was characterized by 1H NMR (300 MHz, CDCl3): δ 8.48-8.84 (m, 1H), 8.94-9.31 (m, 1H). eSI/MS analysis showed m/e of 267 [(M-I)? , 100]. Synthesis of intermediate 7 (Method 2): 6-(3-methoxyphenyl)-5-phenylpyridin-3-amine. Step A: 3-bromo-5-nitropyridin-2-ol, POBr3 and PBr3 were heated and reacted at 120 °C for 3.5 hours. After completion of the reaction, the crude product was poured into an ice-water mixture and extracted with dichloromethane (DCM). The crude product was purified by fast chromatography on SiO2, eluting using a solvent mixture of hexane/ethyl acetate to give 2.63 g of the target product (73% yield). The 1H NMR (300 MHz, DMSO-d6) data of the product were: δ 8.95 (s, 1H), 9.18 (s, 1H).
References
[1] Patent: WO2009/21696, 2009, A1. Location in patent: Page/Page column 42; 45
[2] Journal of the American Chemical Society, 1955, vol. 77, p. 6053
[3] Patent: WO2016/46782, 2016, A1. Location in patent: Page/Page column 123; 124
[4] Patent: US9604978, 2017, B2. Location in patent: Page/Page column 254
2,3-DIBROMO-5-NITRO PYRIDINE Preparation Products And Raw materials
Raw materials
Preparation Products
Supplier | Tel | Country | ProdList | Advantage | |
---|---|---|---|---|---|
Capot Chemical Co.,Ltd. | +8613336195806 | sales@capot.com | China | 29733 | 60 |
career henan chemical co | +86-0371-86658258 +8613203830695 | sales@coreychem.com | China | 29855 | 58 |
Nanjing Dolon Biotechnology Co.,Ltd. | 18905173768 | sales@dolonchem.com | CHINA | 2972 | 58 |
Hubei Jusheng Technology Co.,Ltd. | 18871490254 | linda@hubeijusheng.com | CHINA | 28172 | 58 |
Accela ChemBio Inc. | +1-858-6993322 | info@accelachem.com | United States | 21193 | 58 |
Alchem Pharmtech,Inc. | 8485655694 | sales@alchempharmtech.com | United States | 63687 | 58 |
CONIER CHEM AND PHARMA LIMITED | +8618523575427 | sales@conier.com | China | 49730 | 58 |
Guangzhou Yuheng Pharmaceutical Technology Co., Ltd | +8613580539051 | joe@yuhengpharm.com | CHINA | 21142 | 58 |
SIMAGCHEM CORP | +86-5922680277 +86-13806087780 | sale@simagchem.com | China | 17346 | 58 |
Hefei TNJ Chemical Industry Co.,Ltd. | +86-0551-65418671 +8618949823763 | sales@tnjchem.com | China | 34563 | 58 |
View Lastest Price from 2,3-DIBROMO-5-NITRO PYRIDINE manufacturers
Image | Update time | Product | Price | Min. Order | Purity | Supply Ability | Manufacturer | |
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2021-09-09 | 2,3-DIBROMO-5-NITRO PYRIDINE
15862-36-9
|
US $1.10 / g | 1g | 99.00% | 100 Tons min | Dideu Industries Group Limited | |
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2019-07-12 | 2,3-DIBROMO-5-NITRO PYRIDINE
15862-36-9
|
US $1.00 / KG | 1KG | 99% | 1ton | Career Henan Chemical Co |
-
- 2,3-DIBROMO-5-NITRO PYRIDINE
15862-36-9
- US $1.10 / g
- 99.00%
- Dideu Industries Group Limited
-
- 2,3-DIBROMO-5-NITRO PYRIDINE
15862-36-9
- US $1.00 / KG
- 99%
- Career Henan Chemical Co