- 1-Chloro-3-iodobenzene
-
- $100.00 / 1KG
-
2025-09-25
- CAS:625-99-0
- Min. Order: 1KG
- Purity: 99%
- Supply Ability: g-kg-tons, free sample is available
- 1-Chloro-3-iodobenzene
-
- $0.00 / 25KG
-
2025-08-08
- CAS:625-99-0
- Min. Order: 1KG
- Purity: 99%
- Supply Ability: 50000KG/month
- 1-Chloro-3-iodobenzene
-
- $30.00 / 1kg
-
2025-04-15
- CAS:625-99-0
- Min. Order: 1kg
- Purity: 99%
- Supply Ability: 5000kg/week
|
| 1-Chloro-3-iodobenzene Basic information |
| 1-Chloro-3-iodobenzene Chemical Properties |
Hazard Codes | Xi | Risk Statements | 36/37/38 | Safety Statements | 24/25 | WGK Germany | 3 | TSCA | T | HazardClass | IRRITANT | HS Code | 29039990 |
| 1-Chloro-3-iodobenzene Usage And Synthesis |
Chemical Properties | Clear light yellow liquid | Uses | suzuki reaction | Uses | 1-Chloro-3-iodobenzene is used as a pharmaceutical intermediate. | Synthesis Reference(s) | Synthetic Communications, 11, p. 639, 1981 DOI: 10.1080/00397918108063637 | General Description | The multiple-quantum proton NMR spectra of 3-chloroiodobenzene was studied. | Synthesis | General procedure for the synthesis of m-chloroiodobenzene from 3-chlorophenylboronic acid: a mixture of arylboronic acid (0.55 mmol), KF (96 mg, 1.65 mmol) and I2 (127 mg, 0.50 mmol) in 1,4-dioxane (5 mL) was stirred and reacted for 1 hr at 80 °C. After completion of the reaction, the mixture was filtered through a silica gel column and eluted with ether (10 mL). Subsequently, the solvent was removed by rotary evaporator. For further purification, the target product, m-chloroiodobenzene, was isolated by silica gel column chromatography using petroleum ether/ether (98:2) as eluent. | References | [1] Chemistry - A European Journal, 2011, vol. 17, # 20, p. 5652 - 5660 [2] Tetrahedron Letters, 2015, vol. 56, # 9, p. 1122 - 1123 [3] Synlett, 1998, # 2, p. 141 - 142 [4] Synlett, 2014, vol. 25, # 7, p. 995 - 1000 |
| 1-Chloro-3-iodobenzene Preparation Products And Raw materials |
|