1-Chloro-3-iodobenzene

1-Chloro-3-iodobenzene Suppliers list

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Tel:	+86-371-86557731 +86-13613820652
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Products Intro:	Product Name:1-Chloro-3-iodobenzene CAS:625-99-0 Purity:99% Package:1KG;100USD\|1000KG;1USD

Company Name:	Hebei Zhuanglai Chemical Trading Co.,Ltd
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Products Intro:	Product Name:1-Chloro-3-iodobenzene CAS:625-99-0 Purity:99% Package:1kg;30USD

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Products Intro:	Product Name:1-Chloro-3-iodobenzene CAS:625-99-0 Purity:98% Package:1KG;1USD

1-Chloro-3-iodobenzene manufacturers

1-Chloro-3-iodobenzene Basic information

Product Name:	1-Chloro-3-iodobenzene
Synonyms:	1-Chloro-3-iodobenzene, 98% clear colourless to pale yellow or pale pink liquid;oroiodobenzene;1-chloro-3-iodo-benzen;3-Chloro-1-iodobenzene;3-Iodochlorobenzene;m-Chlorophenyl iodide;M-CHLOROIODOBENZENE;3-CHLOROIODOBENZENE
CAS:	625-99-0
MF:	C6H4ClI
MW:	238.45
EINECS:	210-920-6
Product Categories:	alkyl Iodine\| alkyl chloride;Aromatic Halides (substituted);Chlorine Compounds;Iodine Compounds;Aryl;Halogenated Hydrocarbons;C6
Mol File:	625-99-0.mol

1-Chloro-3-iodobenzene Chemical Properties

Melting point	95-96 °C
Boiling point	103-104 °C15 mm Hg(lit.)
density	1.926 g/mL at 25 °C(lit.)
refractive index	n20/D 1.631(lit.)
Fp	215 °F
storage temp.	Keep in dark place,Sealed in dry,Room Temperature
form	Liquid
Specific Gravity	1.926
color	Clear light yellow
Water Solubility	Soluble in water 67.2 mg/L.
Sensitive	Light Sensitive
BRN	1904539
CAS DataBase Reference	625-99-0(CAS DataBase Reference)
NIST Chemistry Reference	Benzene, 1-chloro-3-iodo-(625-99-0)
EPA Substance Registry System	Benzene, 1-chloro-3-iodo- (625-99-0)

Safety Information

MSDS Information

1-Chloro-3-iodobenzene Usage And Synthesis

Chemical Properties	Clear light yellow liquid
Uses	suzuki reaction
Uses	1-Chloro-3-iodobenzene is used as a pharmaceutical intermediate.
Synthesis Reference(s)	Synthetic Communications, 11, p. 639, 1981 DOI: 10.1080/00397918108063637
General Description	The multiple-quantum proton NMR spectra of 3-chloroiodobenzene was studied.
Synthesis	63503-60-6 625-99-0 General procedure for the synthesis of m-chloroiodobenzene from 3-chlorophenylboronic acid: a mixture of arylboronic acid (0.55 mmol), KF (96 mg, 1.65 mmol) and I2 (127 mg, 0.50 mmol) in 1,4-dioxane (5 mL) was stirred and reacted for 1 hr at 80 °C. After completion of the reaction, the mixture was filtered through a silica gel column and eluted with ether (10 mL). Subsequently, the solvent was removed by rotary evaporator. For further purification, the target product, m-chloroiodobenzene, was isolated by silica gel column chromatography using petroleum ether/ether (98:2) as eluent.
References	[1] Chemistry - A European Journal, 2011, vol. 17, # 20, p. 5652 - 5660 [2] Tetrahedron Letters, 2015, vol. 56, # 9, p. 1122 - 1123 [3] Synlett, 1998, # 2, p. 141 - 142 [4] Synlett, 2014, vol. 25, # 7, p. 995 - 1000

1-Chloro-3-iodobenzene Preparation Products And Raw materials

Raw materials	3-chlorobenzenediazonium tetrafluorborate-->3-Chlorophenylboronic acid-->3-Chlorobenzoic acid-->Potassium fluoride-->iodine-->1,4-Dioxane
Preparation Products	3-Chlorobenzaldehyde-->1-(3-Chlorphenyl)piperazine-->1-Chloro-3-ethylbenzene-->3-Chlorophenoxyacetic acid-->3-CHLOROPHENYLBORONIC ACID, PINACOL ESTER-->Methyl 3-chlorobenzoate-->3-(3-CHLOROPHENYL)PROP-2-YN-1-OL

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