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| | 3-METHOXY-5-METHYLPHENOL Basic information |
| | 3-METHOXY-5-METHYLPHENOL Chemical Properties |
| Melting point | 59-63 °C (lit.) | | Boiling point | 259 °C(Press: 755 Torr) | | density | 1.1106 g/cm3(Temp: 15 °C) | | storage temp. | RT, stored under nitrogen | | solubility | Very slightly soluble in water, soluble in alcohol and oils | | pka | 9.70±0.10(Predicted) | | form | powder to crystal | | color | White to Almost white | | Specific Gravity | 1.11 | | Odor | at 10.00 % in dipropylene glycol. oakmoss fruity iodine woody hay | | Odor Type | mossy | | Cosmetics Ingredients Functions | PERFUMING | | InChI | InChI=1S/C8H10O2/c1-6-3-7(9)5-8(4-6)10-2/h3-5,9H,1-2H3 | | InChIKey | NOTCZLKDULMKBR-UHFFFAOYSA-N | | SMILES | C1(O)=CC(C)=CC(OC)=C1 | | LogP | 2.385 (est) | | CAS DataBase Reference | 3209-13-0(CAS DataBase Reference) | | EPA Substance Registry System | Phenol, 3-methoxy-5-methyl- (3209-13-0) |
| Hazard Codes | Xi | | Risk Statements | 36/37/38 | | Safety Statements | 26-36/37/39-37/39-37 | | WGK Germany | 2 | | TSCA | TSCA listed | | HS Code | 29095090 | | Storage Class | 11 - Combustible Solids | | Hazard Classifications | Eye Irrit. 2
Skin Irrit. 2
STOT SE 3 |
| | 3-METHOXY-5-METHYLPHENOL Usage And Synthesis |
| Chemical Properties | Crystalline powder | | Uses | 3-Methoxy-5-methylphenol (cas# 3209-13-0) is a compound useful in organic synthesis. | | Definition | ChEBI: 3-Methoxy-5-methylphenol is a member of phenols and a member of methoxybenzenes. | | Synthesis Reference(s) | Organic Syntheses, Coll. Vol. 6, p. 859, 1988
The Journal of Organic Chemistry, 49, p. 1672, 1984 DOI: 10.1021/jo00183a043
Tetrahedron Letters, 11, p. 1327, 1970 | | Synthesis | A solution of anhydrous orcinol (12.4 g,0.1 mole) in dry acetone (100 ml)is refluxed for 4 hr with dimethyl sulphate (10.63 ml，14.2 g,0.112 mole) and ignited potassium carbonate (20 g) under anhydrous conditions. The mixture is filtered in hot, and the inorganic salts are washed with hot acetone(25 ml). The combined acetone solution is distilled. The oily product is purified by column chromatography over silica gel using chloroform as aneluant. Orcinol monomethyl ether is obtained as oil. Yield 4.2 g (30.4%). |
| | 3-METHOXY-5-METHYLPHENOL Preparation Products And Raw materials |
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