5-Nitroanthranilonitrile

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Products Intro:	Product Name:2-Cyano-4-nitroaniline CAS:17420-30-3

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Products Intro:	Product Name:5-Nitroanthranilonitrile CAS:17420-30-3 Purity:0.99 Package:5KG;1KG

5-Nitroanthranilonitrile manufacturers

5-Nitroanthranilonitrile Basic information

Product Name:	5-Nitroanthranilonitrile
Synonyms:	2-Cyan-4-nitroaniline;2-cyano-4-nitro-anilin;2-kyan-4-nitroanilin;5-NITROANTHRANILONITRILE;5-nitro-anthranilonitril;2-amino-5-nitro-benzonitril;2-CYANO-4-NITROANILINE;2-AMINO-5-NITROBENZONITRILE
CAS:	17420-30-3
MF:	C7H5N3O2
MW:	163.13
EINECS:	241-446-8
Product Categories:	Aromatic Nitriles;Building Blocks;C6 to C7;Chemical Synthesis;Cyanides/Nitriles;Nitrogen Compounds;Organic Building Blocks;john's
Mol File:	17420-30-3.mol

5-Nitroanthranilonitrile Chemical Properties

Melting point	200-207 °C(lit.)
Boiling point	290.19°C (rough estimate)
density	1.4141 (rough estimate)
refractive index	1.5500 (estimate)
Fp	234 °C
storage temp.	Keep in dark place,Inert atmosphere,Room temperature
solubility	DMSO (Slightly)
pka	-1.97±0.10(Predicted)
form	Solid
color	Dark Yellow
BRN	1425714
InChI	InChI=1S/C7H5N3O2/c8-4-5-3-6(10(11)12)1-2-7(5)9/h1-3H,9H2
InChIKey	MGCGMYPNXAFGFA-UHFFFAOYSA-N
SMILES	C(#N)C1=CC([N+]([O-])=O)=CC=C1N
CAS DataBase Reference	17420-30-3(CAS DataBase Reference)
EPA Substance Registry System	Benzonitrile, 2-amino-5-nitro- (17420-30-3)

Safety Information

Hazard Codes	Xn
Risk Statements	20/21/22-36/37/38
Safety Statements	22-24/25-36-26
WGK Germany	2
RTECS	BX2500000
TSCA	TSCA listed
HS Code	29269090
Storage Class	11 - Combustible Solids
Toxicity	mouse,LD50,oral,6710mg/kg (6710mg/kg),Gigiena Truda i Professional'nye Zabolevaniya. Labor Hygiene and Occupational Diseases. Vol. 30(1), Pg. 50, 1986.

MSDS Information

5-Nitroanthranilonitrile Usage And Synthesis

Chemical Properties	yellow to brownish powder. 2-Amino-5-nitrobenzonitrile [17420-30-3], 2-cyano-4-nitroaniline, Mr 163.13, mp 210℃, is readily soluble in acetone, chloroform, and benzene; it is sparingly soluble in water and ethanol. As already mentioned, the reaction of 2-chloro5-nitrobenzonitrile with ammonia gives 2-amino-5-nitrobenzonitrile, an intermediate for azo dyes.
Production Methods	A newer synthetic route starts from 6-nitroisatoic anhydride [2H-3,1-benzoxazine-6-nitro-2,4 (1H)-dione]: the latter is converted into 2-amino-5-nitrobenzonitrile by reaction with ammonia, subsequent treatment with phosgene in dimethylformamide or Nmethylpyrrolidone, followed by hydrolysis of the formamidine.
Synthesis Reference(s)	Journal of the American Chemical Society, 82, p. 3152, 1960 DOI: 10.1021/ja01497a043
References	[1] Bioorganic and Medicinal Chemistry Letters, 2016, vol. 26, # 11, p. 2589 - 2593

5-Nitroanthranilonitrile Preparation Products And Raw materials

Raw materials	2-Chlorobenzonitrile-->2-Chloro-5-nitrobenzonitrile-->2,2,2-TRIFLUORO-N-(4-NITRO-2-IODOPHENYL)ACETAMIDE-->3-(hydroxyamino)-5-nitroindol-2-one-->1-Pyrrolidinecarbodithioic acid, azanyl ester-->Benzonitrile, 2-amino-3-nitro--->2,5-Diaminobenzonitrile-->2-Iodo-4-nitroaniline-->5-Nitroisatin-->4-Amino-3-nitrobenzonitrile
Preparation Products	6-Nitro-quinazolin-4-ylamine-->EHT 5372-->2-IODO-5-NITROBENZOIC ACID-->2-Amino-5-nitrobenzophenone-->[2-[[4-[(2-cyano-4-nitrophenyl)azo]phenyl]ethylamino]ethyl]trimethylammonium methyl sulphate-->C.I.Disperse Violet 40-->Disperse Red 82-->Disperse Red 107-->Disperse Red 73

Tag:5-Nitroanthranilonitrile(17420-30-3) Related Product Information

2-Methyl-4-nitroaniline ALTRENOGEST 3,4-Dichloroaniline 3-Aminophenol 6-Aminocaproic acid N-Methyl-4-nitroaniline Tris(hydroxymethyl)aminomethane Glycine 4-Chloro-2-nitroaniline 4-Nitroaniline Disperse Violet 33 2-Amino-3-bromo-5-nitrobenzonitrile Disperse Blue 165 Disperse Red 73 2-Amino-3-chloro-5-nitrobenzonitrile Disperse Blue 183 2-(2-HYDROXYETHYLAMINO)-5-NITROBENZONITRILE 3-Nitroaniline

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